N-fluoro-(3,5-di-tert-butyl-4-methoxy)-benzenesulfonimide

Base Information

Chemical Name:N-fluoro-(3,5-di-tert-butyl-4-methoxy)-benzenesulfonimide
CAS No.:1297500-44-7
Molecular Formula:C₃₀H₄₆FNO₆S₂
Molecular Weight:599.829
Hs Code.:

Synonyms:

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Chemical Property of N-fluoro-(3,5-di-tert-butyl-4-methoxy)-benzenesulfonimide

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Technology Process of N-fluoro-(3,5-di-tert-butyl-4-methoxy)-benzenesulfonimide

There total 4 articles about N-fluoro-(3,5-di-tert-butyl-4-methoxy)-benzenesulfonimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1297500-51-6
C₃₀H₄₇NO₆S₂

: 1297500-44-7
N-fluoro-(3,5-di-tert-butyl-4-methoxy)-benzenesulfonimide

Guidance literature:: With fluorine; sodium fluoride; In nitrogen; acetonitrile; at -40 ℃; for 0.166667h;
DOI:10.1016/j.jfluchem.2011.01.005

Reference yield:

: 1297500-47-0
C₁₅H₂₅NO₃S

: 1297500-44-7
N-fluoro-(3,5-di-tert-butyl-4-methoxy)-benzenesulfonimide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran / 0 - 20 °C

2: fluorine; sodium fluoride / nitrogen; acetonitrile / 0.17 h / -40 °C

With sodium hydride; fluorine; sodium fluoride; In tetrahydrofuran; nitrogen; acetonitrile;
DOI:10.1016/j.jfluchem.2011.01.005

Reference yield:

: 1516-95-6
2,6-di-tert-butyl-anisole

: 1297500-44-7
N-fluoro-(3,5-di-tert-butyl-4-methoxy)-benzenesulfonimide

Guidance literature:: Multi-step reaction with 4 steps

1: chlorosulfonic acid / chloroform / 0.17 h / -10 °C

2: ammonium chloride; sodium hydroxide / water; acetone / 4 h / 20 °C

3: sodium hydride / tetrahydrofuran / 0 - 20 °C

4: fluorine; sodium fluoride / nitrogen; acetonitrile / 0.17 h / -40 °C

With chlorosulfonic acid; sodium hydride; fluorine; ammonium chloride; sodium fluoride; sodium hydroxide; In tetrahydrofuran; chloroform; nitrogen; water; acetone; acetonitrile;
DOI:10.1016/j.jfluchem.2011.01.005