2-N-acetyl-3,4-di-O-benzyl-α-D-glucosaminopyranosyl-(1→3)-2-N-acetyl-4-O-benzyl-6-(5-(benzyl((benzyloxy)carbonyl)amino)pentyl (2-cyanoethyl) phosphoryl)-α-D-glucosaminopyranosyl-(1→2)-benzyl (2R)-3-benzyloxypropanoate

Base Information

• Chemical Name: 2-N-acetyl-3,4-di-O-benzyl-α-D-glucosaminopyranosyl-(1→3)-2-N-acetyl-4-O-benzyl-6-(5-(benzyl((benzyloxy)carbonyl)amino)pentyl (2-cyanoethyl) phosphoryl)-α-D-glucosaminopyranosyl-(1→2)-benzyl (2R)-3-benzyloxypropanoate
• CAS No.: 1448013-21-5
• Molecular Formula: C₇₇H₈₉N₄O₁₉P
• Molecular Weight: 1405.54

Synonyms:

Chemical Property of 2-N-acetyl-3,4-di-O-benzyl-α-D-glucosaminopyranosyl-(1→3)-2-N-acetyl-4-O-benzyl-6-(5-(benzyl((benzyloxy)carbonyl)amino)pentyl (2-cyanoethyl) phosphoryl)-α-D-glucosaminopyranosyl-(1→2)-benzyl (2R)-3-benzyloxypropanoate

Chemical Property:

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Useful:

Technology Process of 2-N-acetyl-3,4-di-O-benzyl-α-D-glucosaminopyranosyl-(1→3)-2-N-acetyl-4-O-benzyl-6-(5-(benzyl((benzyloxy)carbonyl)amino)pentyl (2-cyanoethyl) phosphoryl)-α-D-glucosaminopyranosyl-(1→2)-benzyl (2R)-3-benzyloxypropanoate

There total 1 articles about 2-N-acetyl-3,4-di-O-benzyl-α-D-glucosaminopyranosyl-(1→3)-2-N-acetyl-4-O-benzyl-6-(5-(benzyl((benzyloxy)carbonyl)amino)pentyl (2-cyanoethyl) phosphoryl)-α-D-glucosaminopyranosyl-(1→2)-benzyl (2R)-3-benzyloxypropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C80H93N4O19P → 2-N-acetyl-3,4-di-O-benzyl-α-D-glucosaminopyranosyl-(1→3)-2-N-acetyl-4-O-benzyl-6-(5-(benzyl((benzyloxy)carbonyl)amino)pentyl (2-cyanoethyl) phosphoryl)-α-D-glucosaminopyranosyl-(1→2)-benzyl (2R)-3-benzyloxypropanoate (1448013-21-5)

Guidance literature:

With iodine; In tetrahydrofuran; water; acetonitrile; for 3h; Molecular sieve;

DOI:10.1039/c3cc43545h

Reference yield:

2-N-acetyl-3,4-di-O-benzyl-6-O-prop-1-en-α-D-glucosaminopyranosyl-(1→3)-2-N-acetyl-4-O-benzyl-6-((N,N,-diisopropylamino)-2-cyanoethylphosphite)-α-D-glucosaminopyranosyl-(1→2)-benzyl (2R)-3-benzyloxypropanoate (1448013-24-8) + 2-N-acetyl-3,4-di-O-benzyl-α-D-glucosaminopyranosyl-(1→3)-2-N-acetyl-4-O-benzyl-6-(5-(benzyl((benzyloxy)carbonyl)amino)pentyl (2-cyanoethyl) phosphoryl)-α-D-glucosaminopyranosyl-(1→2)-benzyl (2R)-3-benzyloxypropanoate (1448013-21-5) → C137H157N7O35P2

Guidance literature:

With 5-(ethylthio)-1H-tetrazole; In acetonitrile; for 1h; Molecular sieve;

DOI:10.1039/c3cc43545h

Reference yield:

2-N-acetyl-3,4-di-O-benzyl-α-D-glucosaminopyranosyl-(1→3)-2-N-acetyl-4-O-benzyl-6-(5-(benzyl((benzyloxy)carbonyl)amino)pentyl (2-cyanoethyl) phosphoryl)-α-D-glucosaminopyranosyl-(1→2)-benzyl (2R)-3-benzyloxypropanoate (1448013-21-5) + triethylamine (121-44-8) → C74H85N3O19P(1-)*C6H16N(1+)

Guidance literature:

for 16h;

DOI:10.1039/c3cc43545h

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