di-μ-chlorobis[2-(3',5'-dimethyl-1'-pyrazolyl)phenyl-N',C]dipalladium

Base Information

Chemical Name:di-μ-chlorobis[2-(3',5'-dimethyl-1'-pyrazolyl)phenyl-N',C]dipalladium
CAS No.:41707-88-4
Molecular Formula:C₂₂H₂₂Cl₂N₄Pd₂
Molecular Weight:626.189
Hs Code.:

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Chemical Property of di-μ-chlorobis[2-(3',5'-dimethyl-1'-pyrazolyl)phenyl-N',C]dipalladium

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Technology Process of di-μ-chlorobis[2-(3',5'-dimethyl-1'-pyrazolyl)phenyl-N',C]dipalladium

There total 1 articles about di-μ-chlorobis[2-(3',5'-dimethyl-1'-pyrazolyl)phenyl-N',C]dipalladium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1131-16-4
3,5-dimethyl-1-phenyl-1H-pyrazole

: 10025-98-6
potassium tetrachloropalladate(II)

: 870467-01-9,39003-78-6
dichlorobis(3,5-dimethyl-1-phenylpyrazole-N₂)palladium

: 41707-88-4
di-μ-chlorobis[2-(3',5'-dimethyl-1'-pyrazolyl)phenyl-N',C]dipalladium

Guidance literature:: In 1,4-dioxane; water; under N2; mixt. of Pd complex and ligand in aq. dioxane stirred at room temp. for 18 h; heated under reflux for 36 h; filtered, ppt. washed (MeOH, ether), dried, suspn. in CH2Cl2 refluxed (6h), solid washed (CH2Cl2, ether), dried, recrystd. from DMF-MeOH (dimer ); filtrate evapd. to dryness, dissolved in CH2Cl2, filtered, crystd. byadding hexane (monomer); elem. anal.;
DOI:10.1139/v05-110