C₁₆H₂₂O₄

Base Information

Chemical Name:C₁₆H₂₂O₄
CAS No.:1622095-13-9
Molecular Formula:C₁₆H₂₂O₄
Molecular Weight:278.348
Hs Code.:

C<sub>16</sub>H<sub>22</sub>O<sub>4</sub>

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Suppliers and Price of C₁₆H₂₂O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₂₂O₄

Chemical Property:

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Technology Process of C₁₆H₂₂O₄

There total 6 articles about C₁₆H₂₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1622095-41-3
C₂₅H₂₇NO₆

: 1622095-13-9
C₁₆H₂₂O₄

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; water; at 20 ℃; for 18h;
DOI:10.1002/ejoc.201402096

Reference yield:

: 99865-70-0
4-(4-Formyl-phenoxy)butyric acid

: 1622095-13-9
C₁₆H₂₂O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 14 h / 20 °C

2.1: dichloromethane / 23 h / 20 °C

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere

3.2: 11.5 h / -78 - -5 °C

4.1: sodium tetrahydroborate / tetrahydrofuran; water / 18 h / 20 °C

With dmap; sodium tetrahydroborate; sodium hexamethyldisilazane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane; water; 2.1: |Wittig Olefination;
DOI:10.1002/ejoc.201402096

Reference yield:

: 1622095-12-8
C₂₀H₁₉NO₅

: 1622095-13-9
C₁₆H₂₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 23 h / 20 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere

2.2: 11.5 h / -78 - -5 °C

3.1: sodium tetrahydroborate / tetrahydrofuran; water / 18 h / 20 °C

With sodium tetrahydroborate; sodium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water; 1.1: |Wittig Olefination;
DOI:10.1002/ejoc.201402096