[phenyl-2H₄]-2-bromo-N-cumyl benzamide

Base Information

Chemical Name:[phenyl-2H₄]-2-bromo-N-cumyl benzamide
CAS No.:869998-12-9
Molecular Formula:C₁₆H₁₆BrNO
Molecular Weight:322.181
Hs Code.:

[phenyl-2H<sub>4</sub>]-2-bromo-N-cumyl benzamide

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [phenyl-2H₄]-2-bromo-N-cumyl benzamide

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Technology Process of [phenyl-2H₄]-2-bromo-N-cumyl benzamide

There total 3 articles about [phenyl-2H₄]-2-bromo-N-cumyl benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 869998-11-8
[phenyl-2H₅]-N-cumyl benzamide

: 869998-12-9
[phenyl-2H₄]-2-bromo-N-cumyl benzamide

Guidance literature:: [phenyl-2H₅]-N-cumyl benzamide; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; hexane; cyclohexane; at -20 ℃; for 2h;

With ethylene dibromide; In tetrahydrofuran; hexane; cyclohexane; at -20 - 0 ℃;
DOI:10.1002/jlcr.912

Reference yield:

: 43019-90-5
benzoyl chloride-d5

: 869998-12-9
[phenyl-2H₄]-2-bromo-N-cumyl benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 91 percent / triethylamine / tetrahydrofuran / 14 h / 20 °C

2.1: s-BuLi; TMEDA / tetrahydrofuran / 2 h / -20 °C

2.2: 1,2-dibromoethane / tetrahydrofuran / 1 h / -20 °C

With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; triethylamine; In tetrahydrofuran;

Reference yield:

: 585-32-0
2-phenyl-2-propylamine

: 869998-12-9
[phenyl-2H₄]-2-bromo-N-cumyl benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 91 percent / triethylamine / tetrahydrofuran / 14 h / 20 °C

2.1: s-BuLi; TMEDA / tetrahydrofuran / 2 h / -20 °C

2.2: 1,2-dibromoethane / tetrahydrofuran / 1 h / -20 °C

With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; triethylamine; In tetrahydrofuran;