2-amino-4-O-(3,4,6-tri-O-benzyl-2-deoxy-2-dichloroacetamido-β-D-glucopyranosyl)-2-N:3-O-carbonyl-2-deoxy-5,6-isopropylidene-D-glucose diethyl acetal

Base Information

Chemical Name:2-amino-4-O-(3,4,6-tri-O-benzyl-2-deoxy-2-dichloroacetamido-β-D-glucopyranosyl)-2-N:3-O-carbonyl-2-deoxy-5,6-isopropylidene-D-glucose diethyl acetal
CAS No.:70279-97-9
Molecular Formula:C₄₃H₅₄Cl₂N₂O₁₂
Molecular Weight:861.814
Hs Code.:

2-amino-4-O-(3,4,6-tri-O-benzyl-2-deoxy-2-dichloroacetamido-β-D-glucopyranosyl)-2-N:3-O-carbonyl-2-deoxy-5,6-isopropylidene-D-glucose diethyl acetal

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Chemical Property of 2-amino-4-O-(3,4,6-tri-O-benzyl-2-deoxy-2-dichloroacetamido-β-D-glucopyranosyl)-2-N:3-O-carbonyl-2-deoxy-5,6-isopropylidene-D-glucose diethyl acetal

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Technology Process of 2-amino-4-O-(3,4,6-tri-O-benzyl-2-deoxy-2-dichloroacetamido-β-D-glucopyranosyl)-2-N:3-O-carbonyl-2-deoxy-5,6-isopropylidene-D-glucose diethyl acetal

There total 5 articles about 2-amino-4-O-(3,4,6-tri-O-benzyl-2-deoxy-2-dichloroacetamido-β-D-glucopyranosyl)-2-N:3-O-carbonyl-2-deoxy-5,6-isopropylidene-D-glucose diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 18422-15-6
2-amino-2-N:3-O-carbonyl-2-deoxy-5,6-isopropylidene-D-glucose diethyl acetal

: 3,4,6-tri-O-benzyl-2-deoxy-2-dichloroacetamido-D-glucopyranosyl bromide

: 70279-97-9
2-amino-4-O-(3,4,6-tri-O-benzyl-2-deoxy-2-dichloroacetamido-β-D-glucopyranosyl)-2-N:3-O-carbonyl-2-deoxy-5,6-isopropylidene-D-glucose diethyl acetal

Guidance literature:: With mercury(II) cyanide; In benzene; for 24h; Ambient temperature;
DOI:10.1246/bcsj.59.1411

Reference yield:

: 108391-52-2
3,4,6-tri-O-benzyl-2-deoxy-2-dichloroacetamido-α-D-glucopyranosyl p-nitrobenzoate

: 70279-97-9
2-amino-4-O-(3,4,6-tri-O-benzyl-2-deoxy-2-dichloroacetamido-β-D-glucopyranosyl)-2-N:3-O-carbonyl-2-deoxy-5,6-isopropylidene-D-glucose diethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: HBr / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 33 percent / Hg(CN)2 / benzene / 24 h / Ambient temperature

With hydrogen bromide; mercury(II) cyanide; In dichloromethane; benzene;
DOI:10.1246/bcsj.59.1411

Reference yield:

: 108304-72-9
3,4,6-tri-O-benzyl-2-deoxy-2-dichloroacetamido-D-glucopyranose

: 70279-97-9
2-amino-4-O-(3,4,6-tri-O-benzyl-2-deoxy-2-dichloroacetamido-β-D-glucopyranosyl)-2-N:3-O-carbonyl-2-deoxy-5,6-isopropylidene-D-glucose diethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / pyridine; CH₂Cl₂ / 2 h

2: HBr / CH₂Cl₂ / 0.5 h / Ambient temperature

3: 33 percent / Hg(CN)2 / benzene / 24 h / Ambient temperature

With hydrogen bromide; mercury(II) cyanide; In pyridine; dichloromethane; benzene;
DOI:10.1246/bcsj.59.1411