cis-bis[dicyclohexyl(2-methoxyethyl)phosphine-O,P][η(1)-S-sulfur dioxide]rhodium(I) tetraphenylborate

Base Information

Chemical Name:cis-bis[dicyclohexyl(2-methoxyethyl)phosphine-O,P][η(1)-S-sulfur dioxide]rhodium(I) tetraphenylborate
CAS No.:179827-10-2
Molecular Formula:C₂₄H₂₀B*C₃₀H₅₈O₄P₂RhS
Molecular Weight:998.941
Hs Code.:

Synonyms:

Suppliers and Price of cis-bis[dicyclohexyl(2-methoxyethyl)phosphine-O,P][η(1)-S-sulfur dioxide]rhodium(I) tetraphenylborate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of cis-bis[dicyclohexyl(2-methoxyethyl)phosphine-O,P][η(1)-S-sulfur dioxide]rhodium(I) tetraphenylborate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of cis-bis[dicyclohexyl(2-methoxyethyl)phosphine-O,P][η(1)-S-sulfur dioxide]rhodium(I) tetraphenylborate

There total 1 articles about cis-bis[dicyclohexyl(2-methoxyethyl)phosphine-O,P][η(1)-S-sulfur dioxide]rhodium(I) tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 148422-17-7,150026-03-2
[Rh(dicyclohexyl(2-methoxyethyl)phosphine)2][BPh₄]

: 7446-09-5,12143-17-8,89125-89-3
sulfur dioxide

: 179827-10-2
cis-bis[dicyclohexyl(2-methoxyethyl)phosphine-O,P][η(1)-S-sulfur dioxide]rhodium(I) tetraphenylborate

Guidance literature:: In dichloromethane; absence of air and moisture; bubbling SO2 at -40°C, stirring for 5 min; pptn. on hexane addn., drying (vac.); elem. anal.;
DOI:10.1016/0022-328X(95)06038-X

Reference yield: 86.0%

: 179827-10-2
cis-bis[dicyclohexyl(2-methoxyethyl)phosphine-O,P][η(1)-S-sulfur dioxide]rhodium(I) tetraphenylborate

: 80937-33-3
oxygen

: cis-bis[dicyclohexyl(2-methoxyethyl)phosphine-O,P][η(2)-O,O'-sulfate]rhodium(III) tetraphenylborate

Guidance literature:: In dichloromethane; passing O2 at -40°C, stirring for 5 min; pptn. on hexane addn., drying (vac.);
DOI:10.1016/0022-328X(95)06038-X