Benzoic acid, 4-[[2-[[[3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropyl]carbonyl]amino]- 3-methyl-1-oxobutyl]amino]-, ethyl ester

Base Information

Chemical Name:Benzoic acid, 4-[[2-[[[3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropyl]carbonyl]amino]- 3-methyl-1-oxobutyl]amino]-, ethyl ester
CAS No.:111544-74-2
Molecular Formula:C₂₂H₂₈Cl₂N₂O₄
Molecular Weight:455.381
Hs Code.:
Mol file:111544-74-2.mol

Synonyms:

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Chemical Property of Benzoic acid, 4-[[2-[[[3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropyl]carbonyl]amino]- 3-methyl-1-oxobutyl]amino]-, ethyl ester

Chemical Property:

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Technology Process of Benzoic acid, 4-[[2-[[[3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropyl]carbonyl]amino]- 3-methyl-1-oxobutyl]amino]-, ethyl ester

There total 8 articles about Benzoic acid, 4-[[2-[[[3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropyl]carbonyl]amino]- 3-methyl-1-oxobutyl]amino]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.2%

: 52314-67-7,60254-21-9,61914-47-4,66182-41-0,66182-42-1,68539-75-3,69831-14-7,76984-70-8,77026-59-6
1-(R,S)-cis-trans-permetrinic acid chloride

: 4-((S)-2-Amino-3-methyl-butyrylamino)-benzoic acid ethyl ester; hydrobromide

: 111544-74-2,127994-87-0,127994-88-1,127994-95-0,127994-96-1
N-perm-L-valyl-p-aminobenzoic acid ethyl ester

Guidance literature:: With sodium hydrogencarbonate; In ethyl acetate; for 0.5h; Ambient temperature;

Reference yield: 52.0%

: 52314-67-7,60254-21-9,61914-47-4,66182-41-0,66182-42-1,68539-75-3,69831-14-7,76984-70-8,77026-59-6
1-(R,S)-cis-trans-permetrinic acid chloride

: 4-((R)-2-Amino-3-methyl-butyrylamino)-benzoic acid ethyl ester; hydrobromide

: 111544-74-2,127994-87-0,127994-88-1,127994-95-0,127994-96-1
N-perm-D-valyl-p-aminobenzoic acid ethyl ester

Guidance literature:: With sodium hydrogencarbonate; In ethyl acetate; for 0.5h; Ambient temperature;

Reference yield:

: 1685-33-2
N-[(benzyloxy)carbonyl]-D-valine

: 111544-74-2,127994-87-0,127994-88-1,127994-95-0,127994-96-1
N-perm-D-valyl-p-aminobenzoic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine, DCC / CH₂Cl₂ / 4 h / Ambient temperature

2: 20percent HBr / acetic acid / 1 h / Ambient temperature

3: 52 percent / aq. NaHCO₃ / ethyl acetate / 0.5 h / Ambient temperature

With hydrogen bromide; sodium hydrogencarbonate; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; acetic acid; ethyl acetate;