3β-Methoxycholest-4-en-6β-ol acetate

Base Information

• Chemical Name: 3β-Methoxycholest-4-en-6β-ol acetate
• CAS No.: 2701-05-5
• Molecular Formula: C₃₀H₅₀O₃
• Molecular Weight: 458.725
• Mol file: 2701-05-5.mol

Synonyms:

Chemical Property of 3β-Methoxycholest-4-en-6β-ol acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3β-Methoxycholest-4-en-6β-ol acetate

There total 3 articles about 3β-Methoxycholest-4-en-6β-ol acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3β-Methoxy-6β-acetoxy-Δ4-cholesten (2701-05-5)

Guidance literature:

With pyridine; thionyl chloride;

DOI:10.1021/jo50003a014

Reference yield:

6β-acetoxy-3β-methoxycholestan-5α-ol (2868-06-6) → 3β-Methoxy-6β-acetoxy-Δ4-cholesten (2701-05-5)

Guidance literature:

With potassium hydrogensulfate; acetic anhydride;

DOI:10.1002/jlac.19656860120

Reference yield:

→ 3β-Methoxy-Δ4-cholesten-6β-ol-acetat (2701-05-5,57423-70-8)

Guidance literature:

3β-Methoxy-6β-acetoxy-cholestan-5α-ol u. SOCl2 bei 0grad;

upstream raw materials:

6β-acetoxy-3β-methoxycholestan-5α-ol

Refernces

• 1、 Snatzke. "19-nor-5-beta-Methyl steroids. 3. Acetolysis of 3-methoxy steroids". . p. 167 - 181. Retrieved 2007/10/06.