3-phenyl-5,6-dihydro-4H-benzocycl<3.2.2>azine

Base Information

Chemical Name:3-phenyl-5,6-dihydro-4H-benzocycl<3.2.2>azine
CAS No.:102408-91-3
Molecular Formula:C₁₉H₁₅N
Molecular Weight:257.335
Hs Code.:

3-phenyl-5,6-dihydro-4H-benzo<ef>cycl<3.2.2>azine

Synonyms:

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Chemical Property of 3-phenyl-5,6-dihydro-4H-benzocycl<3.2.2>azine

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Technology Process of 3-phenyl-5,6-dihydro-4H-benzocycl<3.2.2>azine

There total 6 articles about 3-phenyl-5,6-dihydro-4H-benzocycl<3.2.2>azine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10500-57-9
5,6,7,8-tetrahydroquinoline

: 102408-91-3
3-phenyl-5,6-dihydro-4H-benzocycl<3.2.2>azine

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / acetone / 1) 2 h, reflux; 2) room temp., overnight

2: 88 percent / NaHCO₃ / ethanol / Heating; overnight

3: 58 percent / Pd/C / toluene / 50 h / Heating

4: 5percent KOH / methanol / 2 h / Heating

5: 400 mg / Cu / quinoline / 10 h / Heating

With potassium hydroxide; copper; sodium hydrogencarbonate; palladium on activated charcoal; In quinoline; methanol; ethanol; acetone; toluene;
DOI:10.1002/jhet.5570220425

Reference yield:

: 102408-79-7
5,6,7,8-tetrahydro-1-phenacylquinolinium bromide

: 102408-91-3
3-phenyl-5,6-dihydro-4H-benzocycl<3.2.2>azine

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / NaHCO₃ / ethanol / Heating; overnight

2: 58 percent / Pd/C / toluene / 50 h / Heating

3: 5percent KOH / methanol / 2 h / Heating

4: 400 mg / Cu / quinoline / 10 h / Heating

With potassium hydroxide; copper; sodium hydrogencarbonate; palladium on activated charcoal; In quinoline; methanol; ethanol; toluene;
DOI:10.1002/jhet.5570220425

Reference yield:

: 120161-18-4
1-phenyl-8,9-dihydro-7H-pyrrolo<3,2,1-ij>quinoline

: 102408-91-3
3-phenyl-5,6-dihydro-4H-benzocycl<3.2.2>azine

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / Pd/C / toluene / 50 h / Heating

2: 5percent KOH / methanol / 2 h / Heating

3: 400 mg / Cu / quinoline / 10 h / Heating

With potassium hydroxide; copper; palladium on activated charcoal; In quinoline; methanol; toluene;
DOI:10.1002/jhet.5570220425