-essigsaeure-methylester

Base Information

• Chemical Name: -essigsaeure-methylester
• CAS No.: 92155-31-2
• Molecular Formula: C₁₃H₂₄O₂
• Molecular Weight: 212.332
• Mol file: 92155-31-2.mol

Synonyms:

Chemical Property of -essigsaeure-methylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of -essigsaeure-methylester

There total 2 articles about -essigsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

<1.8-Dichlor-p-menthyl-(3)>-essigsaeure-methylester (100530-96-9) → -essigsaeure-methylester (92155-31-2)

Guidance literature:

Multistep reaction; (i) (heating in pyridine), (ii) H₂, PtO₂, AcOH;

DOI:10.1039/jr9600003734

Reference yield:

(+/-)-6endo-(α-hydroxy-isopropyl)-1-methyl-2-oxa-bicyclo[3.3.1]nonan-3-one (104851-01-6) → -essigsaeure-methylester (92155-31-2)

Guidance literature:

Multi-step reaction with 2 steps

1: HCl

2: KOH / Pd-C / methanol

With hydrogenchloride; potassium hydroxide; palladium on activated charcoal; In methanol;

DOI:10.1039/jr9600003734

Reference yield:

-essigsaeure-methylester (92155-31-2) + p-toluenesulfonyl chloride (98-59-9) → 1-Methyl-3-ethyl-4-isopropyl-benzol (1198-90-9)

Guidance literature:

Multistep reaction; (i) LiAlH₄, Et₂O, (ii) /BRN= 607898/, Py, (iii) LiAlH₄, THF;

DOI:10.1021/jo01053a014

upstream raw materials:

<1.8-Dichlor-p-menthyl-(3)>-essigsaeure-methylester

(+/-)-6endo-(α-hydroxy-isopropyl)-1-methyl-2-oxa-bicyclo[3.3.1]nonan-3-one

Downstream raw materials:

α-Brom--essigsaeure

1-Methyl-3-ethyl-4-isopropyl-benzol