benzyl 2-acetamido-4-O-(6-acetamido-6-deoxy-β-D-glucopyranosyl)-2-deoxy-3-O--α-D-glucopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-4-O-(6-acetamido-6-deoxy-β-D-glucopyranosyl)-2-deoxy-3-O--α-D-glucopyranoside
CAS No.:83100-80-5
Molecular Formula:C₂₇H₄₀N₂O₁₃
Molecular Weight:600.62
Hs Code.:

benzyl 2-acetamido-4-O-(6-acetamido-6-deoxy-β-D-glucopyranosyl)-2-deoxy-3-O-<D-1-(methoxycarbonyl)ethyl>-α-D-glucopyranoside

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Chemical Property of benzyl 2-acetamido-4-O-(6-acetamido-6-deoxy-β-D-glucopyranosyl)-2-deoxy-3-O--α-D-glucopyranoside

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Technology Process of benzyl 2-acetamido-4-O-(6-acetamido-6-deoxy-β-D-glucopyranosyl)-2-deoxy-3-O--α-D-glucopyranoside

There total 8 articles about benzyl 2-acetamido-4-O-(6-acetamido-6-deoxy-β-D-glucopyranosyl)-2-deoxy-3-O--α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66530-19-6
(R)-2-[(2S,3R,4R,5S,6R)-3-Acetylamino-2-benzyloxy-6-hydroxymethyl-5-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yloxy]-propionic acid methyl ester

: 83100-80-5
benzyl 2-acetamido-4-O-(6-acetamido-6-deoxy-β-D-glucopyranosyl)-2-deoxy-3-O--α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 8 steps

1: p-TsOH*H₂O / dimethylformamide / 2 h / 50 °C

2: pyridine

3: 60percent acetic acid / H₂O / 1 h / 50 °C

4: 310 mg / pyridine / 5 h / -25 °C

5: pyridine

6: 208 mg / sodium azide / dimethylformamide / 6 h / 60 °C

7: 1.) H₂ / 1.) 10percent Pd-C / 1.) methanol, room temperature, 2 h; 2.) methanol, 2 h

8: 99 mg / sodium methoxide / methanol / 0.05 h / Ambient temperature

With pyridine; sodium azide; hydrogen; sodium methylate; toluene-4-sulfonic acid; acetic acid; palladium on activated charcoal; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)82587-2

Reference yield:

: (R)-2-[(2S,3R,4R,5S,6R)-3-Acetylamino-2-benzyloxy-5-((4aR,6S,7R,8R,8aS)-7,8-dihydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-6-hydroxymethyl-tetrahydro-pyran-4-yloxy]-propionic acid methyl ester

: 83100-80-5
benzyl 2-acetamido-4-O-(6-acetamido-6-deoxy-β-D-glucopyranosyl)-2-deoxy-3-O--α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine

2: 60percent acetic acid / H₂O / 1 h / 50 °C

3: 310 mg / pyridine / 5 h / -25 °C

4: pyridine

5: 208 mg / sodium azide / dimethylformamide / 6 h / 60 °C

6: 1.) H₂ / 1.) 10percent Pd-C / 1.) methanol, room temperature, 2 h; 2.) methanol, 2 h

7: 99 mg / sodium methoxide / methanol / 0.05 h / Ambient temperature

With pyridine; sodium azide; hydrogen; sodium methylate; acetic acid; palladium on activated charcoal; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)82587-2

Reference yield:

: C₄₉H₅₃NO₁₉S

: 83100-80-5
benzyl 2-acetamido-4-O-(6-acetamido-6-deoxy-β-D-glucopyranosyl)-2-deoxy-3-O--α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 208 mg / sodium azide / dimethylformamide / 6 h / 60 °C

2: 1.) H₂ / 1.) 10percent Pd-C / 1.) methanol, room temperature, 2 h; 2.) methanol, 2 h

3: 99 mg / sodium methoxide / methanol / 0.05 h / Ambient temperature

With sodium azide; hydrogen; sodium methylate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)82587-2