{methylbis(cyclopentadienyl)titanium(NC-t-Bu)}(BPh₄)

Base Information

Chemical Name:{methylbis(cyclopentadienyl)titanium(NC-t-Bu)}(BPh₄)
CAS No.:109631-01-8
Molecular Formula:C₁₆H₂₂NTi*C₂₄H₂₀B
Molecular Weight:595.471
Hs Code.:

{methylbis(cyclopentadienyl)titanium(NC-t-Bu)}(BPh<sub>4</sub>)

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Chemical Property of {methylbis(cyclopentadienyl)titanium(NC-t-Bu)}(BPh₄)

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Technology Process of {methylbis(cyclopentadienyl)titanium(NC-t-Bu)}(BPh₄)

There total 1 articles about {methylbis(cyclopentadienyl)titanium(NC-t-Bu)}(BPh₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 630-18-2
tert-butyl isocyanide

: 1278-83-7
bis(cyclopentadienyl)methyltitanium(IV) chloride

: 143-66-8
sodium tetraphenyl borate

: 109631-01-8
{methylbis(cyclopentadienyl)titanium(NC-t-Bu)}(BPh₄)

Guidance literature:: In dichloromethane; a soln. of Cp2TiMeCl and t-BuCN in CH2Cl2 was treated with 1 equiv of NaBPh4 at room temp. under Ar, mixt. was stirred for 30 min; nitrile complex was extd. with and recrystd. from CH2Cl2; elem. anal.;

Reference yield: 69.0%

: 630-18-2
tert-butyl isocyanide

: 109631-01-8
{methylbis(cyclopentadienyl)titanium(NC-t-Bu)}(BPh₄)

: 113647-09-9
{bis(cyclopentadienyl)titanium(NCMe-t-Bu)(NC-t-Bu)}(BPh₄)

Guidance literature:: In dichloromethane; Ti-nitrile-complex reacts with excess t-BuCN in CH2Cl2 soln., then mixture is stirred at room temp. under argon for 24 h.; The solvent is removed, extn. of product (CH2Cl2), filtrate is concd., crystd., cooled, elem. anal.;