[Pd(1,2-bis(diphenylphosphino)ethane)(dimethyl sulphoxide)Cl]ClO₄

Base Information

Chemical Name:[Pd(1,2-bis(diphenylphosphino)ethane)(dimethyl sulphoxide)Cl]ClO₄
CAS No.:72476-81-4
Molecular Formula:C₂₈H₃₀ClOP₂PdS*ClO₄
Molecular Weight:717.883
Hs Code.:

[Pd(1,2-bis(diphenylphosphino)ethane)(dimethyl sulphoxide)Cl]ClO<sub>4</sub>

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Chemical Property of [Pd(1,2-bis(diphenylphosphino)ethane)(dimethyl sulphoxide)Cl]ClO₄

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Technology Process of [Pd(1,2-bis(diphenylphosphino)ethane)(dimethyl sulphoxide)Cl]ClO₄

There total 1 articles about [Pd(1,2-bis(diphenylphosphino)ethane)(dimethyl sulphoxide)Cl]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19978-61-1
(1,2-bis(diphenylphosphanyl)ethane)dichloridopalladium(II)

: silver perchlorate

: 67-68-5,8070-53-9
dimethyl sulfoxide

: 72476-81-4
[Pd(1,2-bis(diphenylphosphino)ethane)(dimethyl sulphoxide)Cl]ClO₄

: 72476-84-7
[(Pd(1,2-bis(diphenylphosphino)ethane)Cl)2](ClO₄)2

Guidance literature:: In dichloromethane; dimethyl sulfoxide; byproducts: AgCl; addn. of 1 equiv. AgClO4 (in DMSO) to Pd-complex (in CH2Cl2), stirring (15 min); filtration, partial evapn. (vac.), pptn. on Et2O addn., dissoln. in CH2Cl2, filtration, pptn. on Et2O addn., filtration, washing (EtOH, Et2O), drying in air; elem. anal.; impurity of dimeric complex not sepd., detd. by IR spectroscopy;
DOI:10.1039/DT9790001705