1,9-Decadiyne-3,8-dione, 1,10-diphenyl-

Base Information

Chemical Name:1,9-Decadiyne-3,8-dione, 1,10-diphenyl-
CAS No.:77267-31-3
Molecular Formula:C22H18 O2
Molecular Weight:314.384
Hs Code.:
DSSTox Substance ID:DTXSID60228001
Nikkaji Number:J1.114.723B
Wikidata:Q83107864

Synonyms:BRN 3103811;1,10-Diphenyl-1,9-decadiyne-3,8-dione;1,9-Decadiyne-3,8-dione, 1,10-diphenyl-;77267-31-3;DTXSID60228001;LS-59251

Suppliers and Price of 1,9-Decadiyne-3,8-dione, 1,10-diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 1,9-Decadiyne-3,8-dione, 1,10-diphenyl-

Chemical Property:

Vapor Pressure:1.45E-10mmHg at 25°C
Boiling Point:511.2°C at 760 mmHg
Flash Point:223.7°C
Density:1.14g/cm³
XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:7
Exact Mass:314.130679813
Heavy Atom Count:24
Complexity:496

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C#CC(=O)CCCCC(=O)C#CC2=CC=CC=C2

Technology Process of 1,9-Decadiyne-3,8-dione, 1,10-diphenyl-

There total 5 articles about 1,9-Decadiyne-3,8-dione, 1,10-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 111-50-2
Adipic acid dichloride

: 536-74-3
phenylacetylene

: 77267-31-3
1,10-diphenyl-1,9-decadiyne-3,8-dione

Guidance literature:: With manganese(II) iodide; n-butyllithium; In tetrahydrofuran; hexane; at -20 ℃; for 1h;
DOI:10.1021/jo051403q

Reference yield: 19.0%

: 141-28-6
diethyl adipate

: 536-74-3
phenylacetylene

: 77267-31-3
1,10-diphenyl-1,9-decadiyne-3,8-dione

Guidance literature:: phenylacetylene; With n-butyllithium;

diethyl adipate; With boron trifluoride diethyl etherate;
DOI:10.1055/s-2005-865316

Reference yield: 19.0%

: 141-28-6
diethyl adipate

: 93-89-0,99341-95-4
benzoic acid ethyl ester

: 77267-31-3
1,10-diphenyl-1,9-decadiyne-3,8-dione

Guidance literature:: diethyl adipate; With n-butyllithium;

benzoic acid ethyl ester; With boron trifluoride diethyl etherate; Further stages.;
DOI:10.1055/s-2006-958949