Fe(P(OC₂H₅)2C₆H₅)4(SCHNC₂H₅)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(P(OC₂H₅)2C₆H₅)4(SCHNC₂H₅)][B(C₆H₅)4]

Base Information

• Chemical Name: Fe(P(OC₂H₅)2C₆H₅)4(SCHNC₂H₅)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(P(OC₂H₅)2C₆H₅)4(SCHNC₂H₅)][B(C₆H₅)4]
• CAS No.: 157252-81-8
• Molecular Formula: C₂₄H₂₀B*C₄₃H₆₆FeNO₈P₄S
• Molecular Weight: 1256.04

Synonyms:

Chemical Property of Fe(P(OC₂H₅)2C₆H₅)4(SCHNC₂H₅)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(P(OC₂H₅)2C₆H₅)4(SCHNC₂H₅)][B(C₆H₅)4]

Chemical Property:

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Useful:

Technology Process of Fe(P(OC₂H₅)2C₆H₅)4(SCHNC₂H₅)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(P(OC₂H₅)2C₆H₅)4(SCHNC₂H₅)][B(C₆H₅)4]

There total 1 articles about Fe(P(OC₂H₅)2C₆H₅)4(SCHNC₂H₅)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(P(OC₂H₅)2C₆H₅)4(SCHNC₂H₅)][B(C₆H₅)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Fe(2+)*H(1-)*H2*4P(OC2H5)2C6H5*B(C6H5)4(1-)=[FeH(H2)(P(OC2H5)2C6H5)4][B(C6H5)4] + Ethyl isothiocyanate (542-85-8) → Fe(P(OC2H5)2C6H5)4(SCHNC2H5)(1+)*B(C6H5)4(1-)=[Fe(P(OC2H5)2C6H5)4(SCHNC2H5)][B(C6H5)4] (157252-81-8)

Guidance literature:

In dichloromethane; under an inert atmosphere; EtNCS was added to a soln. of the Fe complexin CH2Cl2 at -80°C, warmed to 0°C over 15 min, stirred for 30 min; solvent was removed at reduced pressure, treated with ethanol, stirred for 30 min, filtered, crystd. from CH2Cl2-ethanol; elem. anal.;

DOI:10.1039/DT9940001769

Reference yield:

Fe(P(OC2H5)2C6H5)4(SCHNC2H5)(1+)*B(C6H5)4(1-)=[Fe(P(OC2H5)2C6H5)4(SCHNC2H5)][B(C6H5)4] (157252-81-8) → Fe(P(OC2H5)2C6H5)3(CO)(SCHNC2H5)(1+)*B(C6H5)4(1-)=[Fe(P(OC2H5)2C6H5)3(CO)(SCHNC2H5)][B(C6H5)4]

Guidance literature:

With CO; In 1,2-dichloro-ethane; under an inert atmosphere; the Fe complex in ClCH2CH2Cl was stirred at room temp. under CO (1 atm) for 3 h; solvent was removed at reduced pressure, treated with ethanol, stirred for 4 h, filtered, crystd. from ethanol; elem. anal.;

DOI:10.1039/DT9940001769

upstream raw materials:

Ethyl isothiocyanate

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