(o-isocyanobenzyl)cyclopentadienyltricarbonylmolybdenum

Base Information

Chemical Name:(o-isocyanobenzyl)cyclopentadienyltricarbonylmolybdenum
CAS No.:91949-14-3
Molecular Formula:C₁₆H₁₁MoNO₃
Molecular Weight:361.208
Hs Code.:

Synonyms:

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Chemical Property of (o-isocyanobenzyl)cyclopentadienyltricarbonylmolybdenum

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Technology Process of (o-isocyanobenzyl)cyclopentadienyltricarbonylmolybdenum

There total 1 articles about (o-isocyanobenzyl)cyclopentadienyltricarbonylmolybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.2%

: 12126-18-0
(η(5)-cyclopentadienyl)tricarbonylmolybdate

: 88644-60-4
o-(iodomethyl)phenyl isocyanide

: 91949-14-3
(o-isocyanobenzyl)cyclopentadienyltricarbonylmolybdenum

Guidance literature:: In 1,2-dimethoxyethane; To a soln. of complex in DME at -78°C was added solid isocyanide, stirred at this temp. for 30 min then slowly warmed to -20°C for 3 h (inert atm.);; evapd. at low temp., dissolved in toluene, passed through Florisil column, concd., pentane was added, cooled to -78°C, crystals were washed with cold pentane and dried under vac.; elem. anal.;;

Reference yield:

: [PdCl₂(triphenylphosphine)]2

: 91949-14-3
(o-isocyanobenzyl)cyclopentadienyltricarbonylmolybdenum

: 91949-05-2
cis-PdCl2(PPh3)(η5-C5H5)Mo(CO)3(o-CH2C6H4NC)

Guidance literature:: In benzene; The mixt. of reagents in C6H6 at room temp. was stirred for 1 h (inert atm.);; concd., Et2O was added, filtered, crystd. from CH2Cl2-Et2O; elem. anal.;;

Reference yield:

: [Pt(μ-Cl)Cl(triphenylphosphine)]2

: 91949-14-3
(o-isocyanobenzyl)cyclopentadienyltricarbonylmolybdenum

: 91949-08-5
cis-PtCl2(PPh3)(η5-C5H5)Mo(CO)3(o-CH2C6H4NC)

Guidance literature:: In benzene; The mixt. of reagents in C6H6 at room temp. was stirred for 1 h (inert atm.);; concd., Et2O was added, filtered, crystd. from CH2Cl2-Et2O; elem. anal.;;