5,6,7,12-tetrahydro-12-oxo-12-phenyldibenz-1,5-thiaphosphocine

Base Information

• Chemical Name: 5,6,7,12-tetrahydro-12-oxo-12-phenyldibenz-1,5-thiaphosphocine
• CAS No.: 68669-02-3
• Molecular Formula: C₂₀H₁₇OPS
• Molecular Weight: 336.394

Synonyms:

Chemical Property of 5,6,7,12-tetrahydro-12-oxo-12-phenyldibenz-1,5-thiaphosphocine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 5,6,7,12-tetrahydro-12-oxo-12-phenyldibenz-1,5-thiaphosphocine

There total 1 articles about 5,6,7,12-tetrahydro-12-oxo-12-phenyldibenz-1,5-thiaphosphocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Bis[o-(bromomethyl)phenyl]phenylphosphine oxide (68669-11-4) → 5,6,7,12-tetrahydro-12-oxo-12-phenyldibenz-1,5-thiaphosphocine (68669-02-3)

Guidance literature:

With sodium hydrogensulfide; In ethanol;

Reference yield:

5,6,7,12-tetrahydro-12-oxo-12-phenyldibenz-1,5-thiaphosphocine (68669-02-3) → C20H17ClPS(1+)*Cl(1-) (109974-65-4)

Guidance literature:

With thionyl chloride; In [D₃]acetonitrile;

DOI:10.1016/S0040-4039(00)85174-6

Reference yield:

5,6,7,12-tetrahydro-12-oxo-12-phenyldibenz-1,5-thiaphosphocine (68669-02-3) → 5,6,7,12-tetrahydro-12-phenyldibenz-1,5-thiaphosphocine

Guidance literature:

With trichlorosilane; In benzene; Ambient temperature;

upstream raw materials:

Bis[o-(bromomethyl)phenyl]phenylphosphine oxide

Downstream raw materials:

12-benzyl-12-phenyl-7,12-dihydro-5H-dibenzo[c,f][1,5]thiaphosphocinium; chloride

C₂₀H₁₇ClPS⁽¹⁺⁾*Cl^(1-)

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