Carbamic acid, [2-oxo-2-[(1-phenylethyl)amino]ethylidene]bis-, dimethyl ester

Base Information

Chemical Name:Carbamic acid, [2-oxo-2-[(1-phenylethyl)amino]ethylidene]bis-, dimethyl ester
CAS No.:74581-14-9
Molecular Formula:C₁₄H₁₉N₃O₅
Molecular Weight:309.322
Hs Code.:
DSSTox Substance ID:DTXSID601139109

Synonyms:DTXSID601139109;Carbamic acid, [2-oxo-2-[(1-phenylethyl)amino]ethylidene]bis-, dimethyl ester;74581-14-9

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Chemical Property of Carbamic acid, [2-oxo-2-[(1-phenylethyl)amino]ethylidene]bis-, dimethyl ester

Chemical Property:

XLogP3:1
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:7
Exact Mass:309.13247072
Heavy Atom Count:22
Complexity:378

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C1=CC=CC=C1)NC(=O)C(NC(=O)OC)NC(=O)OC

Technology Process of Carbamic acid, [2-oxo-2-[(1-phenylethyl)amino]ethylidene]bis-, dimethyl ester

There total 2 articles about Carbamic acid, [2-oxo-2-[(1-phenylethyl)amino]ethylidene]bis-, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 110599-31-0
bismethoxycarbonylacetyl chloride

: 618-36-0
rac-methylbenzylamine

: 74581-14-9
N-(-1-phenylethyl)bismethoxycarbonylaminoacetamide

Guidance literature:: With triethylamine; In dichloromethane; ice-water cooling 20 min.;
DOI:10.1016/S0040-4020(01)89976-2

Reference yield:

: 110599-27-4
bismethoxycarbonylaminoacetic acid

: 74581-14-9
N-(-1-phenylethyl)bismethoxycarbonylaminoacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / PCl₅ / CH₂Cl₂

2: 62 percent / Et₃N / CH₂Cl₂ / ice-water cooling 20 min.

With phosphorus pentachloride; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4020(01)89976-2