C₃₉H₄₁IOPSi⁽¹⁺⁾*I^(1-)

Base Information

• Chemical Name: C₃₉H₄₁IOPSi⁽¹⁺⁾*I^(1-)
• CAS No.: 1195470-57-5
• Molecular Formula: C₃₉H₄₁IOPSi*I
• Molecular Weight: 838.622
• Mol file: 1195470-57-5.mol

Synonyms:

Chemical Property of C₃₉H₄₁IOPSi⁽¹⁺⁾*I^(1-)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₃₉H₄₁IOPSi⁽¹⁺⁾*I^(1-)

There total 1 articles about C₃₉H₄₁IOPSi⁽¹⁺⁾*I^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C21H26I2OSi (1195470-87-1) + triphenylphosphine (603-35-0) → C39H41IOPSi(1+)*I(1-) (1195470-57-5)

Guidance literature:

In ethanol; Heating;

DOI:10.1016/j.tetlet.2009.08.061

Reference yield:

C22H28O2Si (1195470-61-1) + C39H41IOPSi(1+)*I(1-) (1195470-57-5) → C43H53IO2Si2

Guidance literature:

C₃₉H₄₁IOPSi⁽¹⁺⁾*I^(1-); With sodium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 1h;

C₂₂H₂₈O₂Si; In tetrahydrofuran; at -78 - 20 ℃; for 13h;

DOI:10.1016/j.tetlet.2009.08.061

upstream raw materials:

C₂₁H₂₆I₂OSi

triphenylphosphine