H-Gly-3-(Gly)2-OH TFA

Base Information

Chemical Name:H-Gly-3-(Gly)2-OH TFA
CAS No.:96195-03-8
Molecular Formula:C₂HF₃O₂*C₄₅H₅₉N₉O₁₃
Molecular Weight:1048.04
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of H-Gly-3-(Gly)2-OH TFA

Chemical Property:

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Technology Process of H-Gly-3-(Gly)2-OH TFA

There total 2 articles about H-Gly-3-(Gly)2-OH TFA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 96195-29-8
Boc-Gly-3-(Gly)2-OH

: 76-05-1
trifluoroacetic acid

: 96195-03-8
H-Gly-3-(Gly)2-OH TFA

Guidance literature:: In dichloromethane; for 0.5h; Ambient temperature;
DOI:10.1021/jo00213a013

Reference yield:

: 96194-99-9
Boc-Gly-3-(Gly)2-OMe

: 96195-03-8
H-Gly-3-(Gly)2-OH TFA

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / 1 N aq. NaOH / methanol / 4 h / Ambient temperature

2: 98 percent / CH₂Cl₂ / 0.5 h / Ambient temperature

With sodium hydroxide; In methanol; dichloromethane;
DOI:10.1021/jo00213a013

Reference yield: 33.0%

: 96195-03-8
H-Gly-3-(Gly)2-OH TFA

: 96195-04-9
cyclo-ε-(benzyloxy)-L-α-amino-δ-adipamidyl)>

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; In dichloromethane; N,N-dimethyl-formamide; 1.) 0 deg C, 1 h, 2.) RT, 4 d;
DOI:10.1021/jo00213a013