C₃₆H₅₆O₅Si

Base Information

Chemical Name:C₃₆H₅₆O₅Si
CAS No.:1421687-81-1
Molecular Formula:C₃₆H₅₆O₅Si
Molecular Weight:596.923
Hs Code.:

C<sub>36</sub>H<sub>56</sub>O<sub>5</sub>Si

Synonyms:

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Chemical Property of C₃₆H₅₆O₅Si

Chemical Property:

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Technology Process of C₃₆H₅₆O₅Si

There total 19 articles about C₃₆H₅₆O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421687-80-0
C₂₀H₃₈O₅

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1421687-81-1
C₃₆H₅₆O₅Si

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at -30 ℃;
DOI:10.1021/ja3116636

Reference yield:

: 63955-78-2
(E, S)-3,7-dimethyl- oct-2-ene-1,6,7-triol

: 1421687-81-1
C₃₆H₅₆O₅Si

Guidance literature:: Multi-step reaction with 17 steps

1.1: toluene-4-sulfonic acid / acetone / 6 h / 0 °C

2.1: triethylamine / tetrahydrofuran / 1 h / -30 °C / Inert atmosphere

3.1: lithium bromide / tetrahydrofuran / 0.5 h / 0 °C

4.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

4.2: 20 °C

5.1: sodium hydroxide / tetrahydrofuran / 5 h / Reflux

5.2: 0 °C

6.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

6.2: 20 °C

7.1: methanesulfonamide; AD-mix β / tert-butyl alcohol; water / 0 °C

8.1: toluene-4-sulfonic acid / dichloromethane / 20 °C

9.1: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -78 °C / Inert atmosphere

10.1: triethylamine / tetrahydrofuran / 1 h / Inert atmosphere

11.1: lithium bromide / tetrahydrofuran / 0.5 h / 0 °C

12.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

12.2: 20 °C

13.1: sodium hydroxide / tetrahydrofuran / 5 h / 0 °C / Reflux

14.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

14.2: 20 °C

15.1: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -78 °C / Inert atmosphere

16.1: trifluoroacetic acid / methanol; water / 20 °C

17.1: 1H-imidazole / N,N-dimethyl-formamide / -30 °C

With 1H-imidazole; methanesulfonamide; AD-mix β; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; triethylamine; trifluoroacetic acid; lithium bromide; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol;
DOI:10.1021/ja3116636

Reference yield:

: C₁₉H₃₂O₅

: 1421687-81-1
C₃₆H₅₆O₅Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium hydroxide / tetrahydrofuran / 5 h / Reflux

1.2: 0 °C

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

2.2: 20 °C

3.1: methanesulfonamide; AD-mix β / tert-butyl alcohol; water / 0 °C

4.1: toluene-4-sulfonic acid / dichloromethane / 20 °C

5.1: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -78 °C / Inert atmosphere

6.1: triethylamine / tetrahydrofuran / 1 h / Inert atmosphere

7.1: lithium bromide / tetrahydrofuran / 0.5 h / 0 °C

8.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

8.2: 20 °C

9.1: sodium hydroxide / tetrahydrofuran / 5 h / 0 °C / Reflux

10.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

10.2: 20 °C

11.1: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -78 °C / Inert atmosphere

12.1: trifluoroacetic acid / methanol; water / 20 °C

13.1: 1H-imidazole / N,N-dimethyl-formamide / -30 °C

With 1H-imidazole; methanesulfonamide; AD-mix β; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; triethylamine; trifluoroacetic acid; lithium bromide; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1021/ja3116636