Technology Process of C63H92N2Ni2O2P2
There total 7 articles about C63H92N2Ni2O2P2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C55H70N2O2;
With
potassium hydride;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
Glovebox;
Cooling;
{methyl(chloro)(trimethylphosphine)2}nickel(II);
In
diethyl ether;
for 28h;
DOI:10.1021/ja4004816
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tert.-butyl lithium / tetrahydrofuran / 1 h / 20 °C / Schlenk technique; Glovebox; Cooling
1.2: 1 h / Cooling; Schlenk technique; Glovebox
1.3: 96 h / 70 °C / Schlenk technique; Glovebox; Sealed tube
2.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / tetrahydrofuran / 4 h / Schlenk technique; Glovebox; Cooling
2.2: 10 h / Schlenk technique; Glovebox; Cooling
3.1: hydrogenchloride / water; methanol / 2 h / Reflux
4.1: toluene-4-sulfonic acid / methanol
5.1: potassium hydride / tetrahydrofuran / 2 h / 20 °C / Glovebox; Cooling
5.2: 28 h
With
hydrogenchloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium; potassium hydride; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; water;
1.3: |Negishi Coupling;
DOI:10.1021/ja4004816
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride / water; methanol / 2 h / Reflux
2.1: toluene-4-sulfonic acid / methanol
3.1: potassium hydride / tetrahydrofuran / 2 h / 20 °C / Glovebox; Cooling
3.2: 28 h
With
hydrogenchloride; potassium hydride; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; water;
DOI:10.1021/ja4004816
