(Me₂Si(C₅Me₄)2)2Th(benzyl alcoholate)2

Base Information

• Chemical Name: (Me₂Si(C₅Me₄)2)2Th(benzyl alcoholate)2
• CAS No.: 1264111-85-4
• Molecular Formula: C₃₄H₄₄O₂SiTh
• Molecular Weight: 744.846
• Mol file: 1264111-85-4.mol

Synonyms:

Chemical Property of (Me₂Si(C₅Me₄)2)2Th(benzyl alcoholate)2

Chemical Property:

Purity/Quality:

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Technology Process of (Me₂Si(C₅Me₄)2)2Th(benzyl alcoholate)2

There total 1 articles about (Me₂Si(C₅Me₄)2)2Th(benzyl alcoholate)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

ansa-Me2SiCp''2Th''Bu2 (89597-07-9) + benzyl alcohol (100-51-6,185532-71-2) → (Me2Si(C5Me4)2)2Th(benzyl alcoholate)2 (1264111-85-4)

Guidance literature:

In toluene; byproducts: butane; (Ar); addn. of 2 equiv. of benzyl alcohol to toluene soln. of thorium compd. at -78°C, stirring for 1 h; replacing toluene by hexane at low temp., filtration at -78.deree.C, elem. anal.;

DOI:10.1021/ja105696p

upstream raw materials:

ansa-Me₂SiCp''2Th''Bu₂

benzyl alcohol