5--2'-deoxyuridine

Base Information

Chemical Name:5--2'-deoxyuridine
CAS No.:108664-92-2
Molecular Formula:C₁₇H₁₈N₂O₇
Molecular Weight:362.339
Hs Code.:

5-<p-(methoxycarbonyl)phenyl>-2'-deoxyuridine

Synonyms:

Suppliers and Price of 5--2'-deoxyuridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5--2'-deoxyuridine

Chemical Property:

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Technology Process of 5--2'-deoxyuridine

There total 3 articles about 5--2'-deoxyuridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-[1-((2R,4S,5R)-4-Acetoxy-5-acetoxymethyl-tetrahydro-furan-2-yl)-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidin-5-yl]-benzoic acid methyl ester

: 108664-92-2
5--2'-deoxyuridine

Guidance literature:: With hydrogenchloride; In methanol; for 12h; Yield given;
DOI:10.1021/jo00392a023

Reference yield:

: 619-44-3
methyl 4-iodobenzoate

: 108664-92-2
5--2'-deoxyuridine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) tetrakis(triphenylphosphine)palladium⁽⁰⁾ / 1.) THF, RT, 15 min, 2.) THF, diglyme, 120 deg C, 12 h

2: HCl(g) / methanol / 12 h

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol;
DOI:10.1021/jo00392a023

Reference yield:

: 92510-77-5
3',5'-di-O-acetyl-5-(chloromercurio)-2'-deoxyuridine

: 108664-92-2
5--2'-deoxyuridine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) tetrakis(triphenylphosphine)palladium⁽⁰⁾ / 1.) THF, RT, 15 min, 2.) THF, diglyme, 120 deg C, 12 h

2: HCl(g) / methanol / 12 h

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol;
DOI:10.1021/jo00392a023