2,2,5,5-TETRAMETHYL-4-METHYLENE-3-FORMYL-IMIDAZOLIDINE-1-OXYL

Base Information

Chemical Name:2,2,5,5-TETRAMETHYL-4-METHYLENE-3-FORMYL-IMIDAZOLIDINE-1-OXYL
CAS No.:82814-77-5
Molecular Formula:C₉H₁₅N₂O₂
Molecular Weight:183.23
Hs Code.:
Mol file:82814-77-5.mol

Synonyms:2,2,5,5-TETRAMETHYL-4-METHYLENE-3-FORMYL-IMIDAZOLIDINE-1-OXYL;2,2,5,5-TETRAMETHYL-4-METHYLENE-3-FORMYL-IMIDAZOLIDINE-1-OXYL FREE RADICAL

Suppliers and Price of 2,2,5,5-TETRAMETHYL-4-METHYLENE-3-FORMYL-IMIDAZOLIDINE-1-OXYL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,2,5,5-TETRAMETHYL-4-METHYLENE-3-FORMYL-IMIDAZOLIDINE-1-OXYL 95.00%
5MG
$ 503.18

Total 6 raw suppliers

Chemical Property of 2,2,5,5-TETRAMETHYL-4-METHYLENE-3-FORMYL-IMIDAZOLIDINE-1-OXYL

Chemical Property:

Vapor Pressure:0.000151mmHg at 25°C
Melting Point:88-93℃
Refractive Index:1.4922 (estimate)
Boiling Point:308.5°C at 760 mmHg
Flash Point:140.4°C
PSA：43.78000
Density:1.13g/cm³
LogP:1.68970
Storage Temp.:0-6°C

Purity/Quality:

98%min ^*data from raw suppliers

2,2,5,5-TETRAMETHYL-4-METHYLENE-3-FORMYL-IMIDAZOLIDINE-1-OXYL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Safety Statements: S24/25:Avoid contact with skin and eyes.;

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,2,5,5-TETRAMETHYL-4-METHYLENE-3-FORMYL-IMIDAZOLIDINE-1-OXYL

There total 1 articles about 2,2,5,5-TETRAMETHYL-4-METHYLENE-3-FORMYL-IMIDAZOLIDINE-1-OXYL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39753-74-7
2,2,4,5,5-pentamethyl-2,5-dihydro-1H-imidazol-1-yloxy

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 82814-77-5
2,2,5,5-tetramethyl-4-methylene-3-formylimidazolidin-1-oxyl

Guidance literature:: With trichlorophosphate;
DOI:10.1007/BF00956013

Reference yield: 15.0%

: 82814-77-5
2,2,5,5-tetramethyl-4-methylene-3-formylimidazolidin-1-oxyl

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 82840-78-6
4-(2-oxoethyliden)-2,2,5,5-tetramethylimidazolidine-1-oxyl

: 119552-86-2
4-(2-N,N-dimethyliminethyliden)-2,2,5,5-tetramethyl-3-formylimidazolidine-1-oxyl chloride

Guidance literature:: With trichlorophosphate; at 20 ℃; for 1h;
DOI:10.1007/BF00755689

Reference yield:

: 82814-77-5
2,2,5,5-tetramethyl-4-methylene-3-formylimidazolidin-1-oxyl

: 3-(Hydroxy-phenyl-methyl)-2,2,5,5-tetramethyl-4-methylene-imidazolidin-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 2.)MnO₂ / 1.)Et₂O, 1 h 2.)20 deg C, 2 h

2: 70 percent / Zn/NH₄Cl / methanol / 0.5 h

With manganese(IV) oxide; ammonium chloride; zinc; In methanol;
DOI:10.1007/BF00755689