6-benzyloxy-(Z)-hex-4-enal oxime

Base Information

Chemical Name:6-benzyloxy-(Z)-hex-4-enal oxime
CAS No.:142404-88-4
Molecular Formula:C₁₃H₁₇NO₂
Molecular Weight:219.283
Hs Code.:

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Chemical Property of 6-benzyloxy-(Z)-hex-4-enal oxime

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Technology Process of 6-benzyloxy-(Z)-hex-4-enal oxime

There total 4 articles about 6-benzyloxy-(Z)-hex-4-enal oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4039-82-1
Benzyl propargyl ether

: 142404-88-4,142404-98-6
6-benzyloxy-(Z)-hex-4-enal oxime

Guidance literature:: Multi-step reaction with 4 steps

1: 1a) BuLi, b) TMEDA / 1a) THF, hexane, 0 deg C, 1.5 h, b) rt, 10 min, 2) reflux, 48 h

2: 91 percent / H₂ / Lindlar catalyst / ethyl acetate / 3 h / 760 Torr / Ambient temperature

3: AcOH / tetrahydrofuran; H₂O / 60 h / 50 °C

4: 1) NaOAc, 2) NH₂OH*HCl / 1) MeOH, 2) 12 h, rt

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; hydroxylamine hydrochloride; hydrogen; sodium acetate; acetic acid; Lindlar's catalyst; In tetrahydrofuran; water; ethyl acetate;

Reference yield:

: 142404-96-4
5-benzyloxypent-3-ynyl-1,3-dioxolane

: 142404-88-4,142404-98-6
6-benzyloxy-(Z)-hex-4-enal oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / H₂ / Lindlar catalyst / ethyl acetate / 3 h / 760 Torr / Ambient temperature

2: AcOH / tetrahydrofuran; H₂O / 60 h / 50 °C

3: 1) NaOAc, 2) NH₂OH*HCl / 1) MeOH, 2) 12 h, rt

With hydroxylamine hydrochloride; hydrogen; sodium acetate; acetic acid; Lindlar's catalyst; In tetrahydrofuran; water; ethyl acetate;

Reference yield:

: 142404-97-5
5-benzyloxy-(Z)-pent-3-enyl-1,3-dioxolane

: 142404-88-4,142404-98-6
6-benzyloxy-(Z)-hex-4-enal oxime

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH / tetrahydrofuran; H₂O / 60 h / 50 °C

2: 1) NaOAc, 2) NH₂OH*HCl / 1) MeOH, 2) 12 h, rt

With hydroxylamine hydrochloride; sodium acetate; acetic acid; In tetrahydrofuran; water;