Technology Process of C15H18O2
There total 4 articles about C15H18O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triphenylstannylcobaloxime; N-ethyl-N,N-diisopropylamine;
In
acetonitrile;
at 50 ℃;
for 16h;
Inert atmosphere;
Sanlamp irradiation;
DOI:10.1002/anie.201105235
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium iodide / acetone / 1.5 h / 0 - 56 °C
2: triphenylstannylcobaloxime; N-ethyl-N,N-diisopropylamine / acetonitrile / 16 h / 50 °C / Inert atmosphere; Sanlamp irradiation
With
triphenylstannylcobaloxime; N-ethyl-N,N-diisopropylamine; sodium iodide;
In
acetone; acetonitrile;
2: Heck-type coupling;
DOI:10.1002/anie.201105235
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium bromide / acetonitrile / 0.5 h / 0 °C / Inert atmosphere
1.2: 1 h / Inert atmosphere
2.1: sodium iodide / acetone / 1.5 h / 0 - 56 °C
3.1: triphenylstannylcobaloxime; N-ethyl-N,N-diisopropylamine / acetonitrile / 16 h / 50 °C / Inert atmosphere; Sanlamp irradiation
With
triphenylstannylcobaloxime; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; sodium iodide; lithium bromide;
In
acetone; acetonitrile;
3.1: Heck-type coupling;
DOI:10.1002/anie.201105235