2-tert-butoxycarbonylamino-4-methyl-pentanoic acid 5-{2-[2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-pentanoylamino]-phenyl}-5-oxo-pentyl ester

Base Information

Chemical Name:2-tert-butoxycarbonylamino-4-methyl-pentanoic acid 5-{2-[2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-pentanoylamino]-phenyl}-5-oxo-pentyl ester
CAS No.:380415-71-4
Molecular Formula:C₄₃H₅₅N₃O₈
Molecular Weight:741.925
Hs Code.:

2-<i>tert</i>-butoxycarbonylamino-4-methyl-pentanoic acid 5-{2-[2-(9<i>H</i>-fluoren-9-ylmethoxycarbonylamino)-4-methyl-pentanoylamino]-phenyl}-5-oxo-pentyl ester

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Chemical Property of 2-tert-butoxycarbonylamino-4-methyl-pentanoic acid 5-{2-[2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-pentanoylamino]-phenyl}-5-oxo-pentyl ester

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Technology Process of 2-tert-butoxycarbonylamino-4-methyl-pentanoic acid 5-{2-[2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-pentanoylamino]-phenyl}-5-oxo-pentyl ester

There total 6 articles about 2-tert-butoxycarbonylamino-4-methyl-pentanoic acid 5-{2-[2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-pentanoylamino]-phenyl}-5-oxo-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13139-15-6,53296-34-7
Boc-DL-Leu-OH

: 380415-71-4
2-tert-butoxycarbonylamino-4-methyl-pentanoic acid 5-{2-[2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-pentanoylamino]-phenyl}-5-oxo-pentyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: DCC; DMAP / CH₂Cl₂

2: dipyridyl carbonate; DMAP / toluene

With dmap; 2,2'-dipyridyl carbonate; dicyclohexyl-carbodiimide; In dichloromethane; toluene;
DOI:10.1021/ol016394w

Reference yield:

: 5390-04-5
pent-1-yn-5-ol

: 380415-71-4
2-tert-butoxycarbonylamino-4-methyl-pentanoic acid 5-{2-[2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-pentanoylamino]-phenyl}-5-oxo-pentyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / [PdCl₂(PPh₃)2]; CuI; Et₂NH

2: 100 percent / Na₂S; HCl / methanol; H₂O

3: DCC; DMAP / CH₂Cl₂

4: dipyridyl carbonate; DMAP / toluene

With hydrogenchloride; dmap; sodium sulfide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 2,2'-dipyridyl carbonate; diethylamine; dicyclohexyl-carbodiimide; In methanol; dichloromethane; water; toluene;
DOI:10.1021/ol016394w

Reference yield:

: 615-43-0
2-iodophenylamine

: 380415-71-4
2-tert-butoxycarbonylamino-4-methyl-pentanoic acid 5-{2-[2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-pentanoylamino]-phenyl}-5-oxo-pentyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / [PdCl₂(PPh₃)2]; CuI; Et₂NH

2: 100 percent / Na₂S; HCl / methanol; H₂O

3: DCC; DMAP / CH₂Cl₂

4: dipyridyl carbonate; DMAP / toluene

With hydrogenchloride; dmap; sodium sulfide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 2,2'-dipyridyl carbonate; diethylamine; dicyclohexyl-carbodiimide; In methanol; dichloromethane; water; toluene;
DOI:10.1021/ol016394w