3-bromo-2-phenylsulfinyl-1-phenylsulfonylindole

Base Information

Chemical Name:3-bromo-2-phenylsulfinyl-1-phenylsulfonylindole
CAS No.:145887-97-4
Molecular Formula:C₂₀H₁₄BrNO₃S₂
Molecular Weight:460.372
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-bromo-2-phenylsulfinyl-1-phenylsulfonylindole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of 3-bromo-2-phenylsulfinyl-1-phenylsulfonylindole

There total 1 articles about 3-bromo-2-phenylsulfinyl-1-phenylsulfonylindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 145887-95-2
3-bromo-1-phenylsulfonyl-2-phenylthioindole

: 145887-97-4
3-bromo-2-phenylsulfinyl-1-phenylsulfonylindole

: 145887-99-6
3-bromo-1,2-diphenylsulfonylindole

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 14h; Ambient temperature;

Reference yield:

: 145887-97-4
3-bromo-2-phenylsulfinyl-1-phenylsulfonylindole

: 145887-94-1
3-bromo-2-deutero-1-phenylsulfonylindole

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) PhMgBr, anthracene, 2.) MeI / 1.) diglyme, Et₂O, reflux, 10 h, 2.) diglyme, Et₂O, overnight

2: 1.) LDA, 2.) CNBr / 1.) THF, heptane, -78 deg C, 40 min, 2.) THF, heptane, RT, overnight

3: 1.) tert-BuLi, 2.) 2,5-dimethylfuran, 3.) D₂O

With 2,5-dimethylfuran; bromocyane; anthracene; water-d2; tert.-butyl lithium; phenylmagnesium bromide; lithium diisopropyl amide; methyl iodide;

Reference yield:

: 145887-97-4
3-bromo-2-phenylsulfinyl-1-phenylsulfonylindole

: 99655-68-2
3-bromo-1-phenylsulfonyl indole

Guidance literature:: With anthracene; phenylmagnesium bromide; methyl iodide; Yield given. Multistep reaction; 1.) diglyme, Et₂O, reflux, 10 h, 2.) diglyme, Et₂O, overnight;