(2S)-2-<oxy>-4-methylpentanoate

Base Information

Chemical Name:(2S)-2-<oxy>-4-methylpentanoate
CAS No.:109638-91-7
Molecular Formula:C₁₄H₂₂NO₅P
Molecular Weight:315.306
Hs Code.:

(2S)-2-<<hydroxy(2-phenyl-1-aminoethyl)phosphinyl>oxy>-4-methylpentanoate

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-2-<oxy>-4-methylpentanoate

Chemical Property:

Purity/Quality:

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Technology Process of (2S)-2-<oxy>-4-methylpentanoate

There total 6 articles about (2S)-2-<oxy>-4-methylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109638-95-1,109638-96-2
(S)-2-[(1-Benzyloxycarbonylamino-2-phenyl-ethyl)-hydroxy-phosphinoyloxy]-4-methyl-pentanoic acid

: 109638-91-7,109638-92-8
(2S)-2-<oxy>-4-methylpentanoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 2.5h; under 760 Torr;
DOI:10.1021/jm00392a014

Reference yield:

: 73270-46-9,132372-69-1,132372-70-4
diphenyl α-N-(benzyloxycarbonyl)amino-2-phenylethylphosphonate

: 109638-91-7,109638-92-8
(2S)-2-<oxy>-4-methylpentanoate

Guidance literature:: Multi-step reaction with 6 steps

1: MeONa / 2 h / 22 °C

2: NaOH / methanol / 4 h / Heating

3: SOCl₂ / CH₂Cl₂ / 3.5 h / 22 °C

4: Et₃N / CH₂Cl₂ / 26 h

5: 65 percent / LiSPr / hexamethylphosphoric acid triamide; tetrahydrofuran / 2 h / 22 °C

6: H₂ / 10percent Pd/C / methanol / 2.5 h / 760 Torr

With sodium hydroxide; thionyl chloride; hydrogen; sodium methylate; lithium n-propylmercaptide; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1021/jm00392a014

Reference yield:

: 84690-42-6
dimethyl 1-benzyloxycarbonylamino-2-phenylethyl phosphonate

: 109638-91-7,109638-92-8
(2S)-2-<oxy>-4-methylpentanoate

Guidance literature:: Multi-step reaction with 5 steps

1: NaOH / methanol / 4 h / Heating

2: SOCl₂ / CH₂Cl₂ / 3.5 h / 22 °C

3: Et₃N / CH₂Cl₂ / 26 h

4: 65 percent / LiSPr / hexamethylphosphoric acid triamide; tetrahydrofuran / 2 h / 22 °C

5: H₂ / 10percent Pd/C / methanol / 2.5 h / 760 Torr

With sodium hydroxide; thionyl chloride; hydrogen; lithium n-propylmercaptide; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1021/jm00392a014