Technology Process of C57H76N10O16S2
There total 7 articles about C57H76N10O16S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 19 h / 20 °C / Inert atmosphere
2.1: N,N-dimethyl-formamide / 30 h / 40 °C / Inert atmosphere
2.2: 3 h / 20 °C / Inert atmosphere; Darkness
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
N,N-dimethyl-formamide;
DOI:10.1039/c4cc04557b
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: Cleland's reagent; triethylamine / tetrahydrofuran; methanol / 3 h / 20 °C / Inert atmosphere
2.1: N,N-dimethyl-formamide / 30 h / 40 °C / Inert atmosphere
2.2: 3 h / 20 °C / Inert atmosphere; Darkness
With
triethylamine; Cleland's reagent;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1039/c4cc04557b
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1,4-dioxane / 21 h / 20 °C / Inert atmosphere
2.1: ethyl acetate / 0.2 h / 20 °C
3.1: acetic anhydride; sodium acetate / 2.5 h / 95 °C
4.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C
4.2: 1.83 h / 0 °C
4.3: 0 °C
5.1: N,N-dimethyl-formamide / 30 h / 40 °C / Inert atmosphere
5.2: 3 h / 20 °C / Inert atmosphere; Darkness
With
sodium acetate; acetic anhydride; trifluoroacetic acid;
In
1,4-dioxane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/c4cc04557b
