Technology Process of C24H30N8O2
There total 7 articles about C24H30N8O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride / 1,4-dioxane / 95 °C
2: hydrogenchloride / ethanol
3: N-ethyl-N,N-diisopropylamine / dichloromethane
With
hydrogenchloride; tris-(dibenzylideneacetone)dipalladium(0); N-ethyl-N,N-diisopropylamine; sodium t-butanolate; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride;
In
1,4-dioxane; ethanol; dichloromethane;
1: Buchwald coupling;
DOI:10.1016/j.bmcl.2010.12.036
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / ethanol
2: N-ethyl-N,N-diisopropylamine / dichloromethane
With
hydrogenchloride; N-ethyl-N,N-diisopropylamine;
In
ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2010.12.036
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 10% palladium on activated charcoal; hydrogen / methanol
2: tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride / 1,4-dioxane / 95 °C
3: hydrogenchloride / ethanol
4: N-ethyl-N,N-diisopropylamine / dichloromethane
With
hydrogenchloride; tris-(dibenzylideneacetone)dipalladium(0); 10% palladium on activated charcoal; hydrogen; N-ethyl-N,N-diisopropylamine; sodium t-butanolate; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride;
In
1,4-dioxane; methanol; ethanol; dichloromethane;
2: Buchwald coupling;
DOI:10.1016/j.bmcl.2010.12.036
