Borane, [(1S,2S)-2-methylcyclohexyl](1,1,2-trimethylpropyl)-

Base Information

Chemical Name:Borane, [(1S,2S)-2-methylcyclohexyl](1,1,2-trimethylpropyl)-
CAS No.:112398-77-3
Molecular Formula:C13H27B
Molecular Weight:194.168
Hs Code.:

Synonyms:

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Chemical Property of Borane, [(1S,2S)-2-methylcyclohexyl](1,1,2-trimethylpropyl)-

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Technology Process of Borane, [(1S,2S)-2-methylcyclohexyl](1,1,2-trimethylpropyl)-

There total 1 articles about Borane, [(1S,2S)-2-methylcyclohexyl](1,1,2-trimethylpropyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 563-79-1
2,3-Dimethyl-2-butene

: 93984-85-1
(2-methylcyclohexyl)borane

: 112398-77-3
(1S,2S)-trans-(2-methylcyclohexyl)thexylborane

Guidance literature:: With chloro-trimethyl-silane; In tetrahydrofuran; byproducts: LiCl; 2,3-Me2-butene added to the (methylcyclohexyl)borane in THF at 0°C together with Me3SiCl; LiCl settled, supernatant sepd.;
DOI:10.1021/ja00213a028

Reference yield:

: 112398-77-3
(1S,2S)-trans-(2-methylcyclohexyl)thexylborane

: 15963-37-8
trans-2-methylcyclohexanol

Guidance literature:: With methanol; Multistep reaction; 2) oxidation;
DOI:10.1021/ja00213a028

Reference yield:

: 109-67-1
1-penten

: 112398-77-3
(1S,2S)-trans-(2-methylcyclohexyl)thexylborane

: (1S,2S)-trans-(2-methylcyclohexyl)(pentyl)thexylborane

Guidance literature:: In tetrahydrofuran; addn. of 1-pentene to (methylhexyl)thexylborane in THF at 0°C, stirring for 2 h; not isolated;
DOI:10.1021/ja00213a028