4-4)-β-D-glucopyranosyl>-3,5-dimethoxyacetonphenone

Base Information

Chemical Name:4-4)-β-D-glucopyranosyl>-3,5-dimethoxyacetonphenone
CAS No.:139906-67-5
Molecular Formula:C₂₂H₃₂O₁₄
Molecular Weight:520.488
Hs Code.:

4-<O-α-D-Glucopyranosyl-(1->4)-β-D-glucopyranosyl>-3,5-dimethoxyacetonphenone

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Chemical Property of 4-4)-β-D-glucopyranosyl>-3,5-dimethoxyacetonphenone

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Technology Process of 4-4)-β-D-glucopyranosyl>-3,5-dimethoxyacetonphenone

There total 2 articles about 4-4)-β-D-glucopyranosyl>-3,5-dimethoxyacetonphenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2478-38-8
1-(4-hydroxy-3,5-dimethoxy-phenyl)-ethanone

: 139906-67-5
4-4)-β-D-glucopyranosyl>-3,5-dimethoxyacetonphenone

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 0.286 M NaOH, 2) pyridine / 1) acetone, r.t., 2) 90 deg C, 50 min.

2: 1M CH₃ONa / methanol / 6 h / Ambient temperature

With pyridine; sodium hydroxide; sodium methylate; In methanol;
DOI:10.1016/S0008-6215(00)90495-6

Reference yield:

: 4753-07-5,5160-10-1,14206-57-6,14227-66-8,14257-35-3,42385-75-1,67650-37-7,68682-05-3,69308-57-2,69349-74-2,70223-96-0,70223-97-1,71276-38-5,85248-99-3,118493-15-5,120575-76-0
2,3,6,2',3',4',6'-hepta-O-acetyl-α-D-maltosyl bromide

: 139906-67-5
4-4)-β-D-glucopyranosyl>-3,5-dimethoxyacetonphenone

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 0.286 M NaOH, 2) pyridine / 1) acetone, r.t., 2) 90 deg C, 50 min.

2: 1M CH₃ONa / methanol / 6 h / Ambient temperature

With pyridine; sodium hydroxide; sodium methylate; In methanol;
DOI:10.1016/S0008-6215(00)90495-6