Technology Process of C34H30N2O4
There total 7 articles about C34H30N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C
1.2: 1 h / -78 °C
2.1: methanesulfonyl chloride; triethylamine / dichloromethane / 4 h / -60 - 0 °C
3.1: hydrogen / methanol / 2 h / 760.05 Torr
4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C
4.2: -78 - 20 °C
5.1: chloroform-d1 / Acidic conditions
With
N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; hydrogen; sodium hexamethyldisilazane; methanesulfonyl chloride; triethylamine;
In
tetrahydrofuran; methanol; chloroform-d1; hexane; dichloromethane;
1.2: |Aldol Condensation;
DOI:10.1016/j.tetlet.2013.05.146
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / Inert atmosphere
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere
2.2: -78 - 0 °C / Inert atmosphere
3.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C
3.2: 1 h / -78 °C
4.1: methanesulfonyl chloride; triethylamine / dichloromethane / 4 h / -60 - 0 °C
5.1: hydrogen / methanol / 2 h / 760.05 Torr
6.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C
6.2: -78 - 20 °C
7.1: chloroform-d1 / Acidic conditions
With
N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; oxalyl dichloride; tetrabutyl ammonium fluoride; hydrogen; sodium hexamethyldisilazane; acetic acid; dimethyl sulfoxide; methanesulfonyl chloride; triethylamine;
In
tetrahydrofuran; methanol; chloroform-d1; hexane; dichloromethane;
2.1: |Swern Oxidation / 2.2: |Swern Oxidation / 3.2: |Aldol Condensation;
DOI:10.1016/j.tetlet.2013.05.146
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: methanesulfonyl chloride; triethylamine / dichloromethane / 4 h / -60 - 0 °C
2.1: hydrogen / methanol / 2 h / 760.05 Torr
3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C
3.2: -78 - 20 °C
4.1: chloroform-d1 / Acidic conditions
With
hydrogen; sodium hexamethyldisilazane; methanesulfonyl chloride; triethylamine;
In
tetrahydrofuran; methanol; chloroform-d1; dichloromethane;
DOI:10.1016/j.tetlet.2013.05.146
