<2R-(2α(R*),3aα,4α,7α,7aα)>-N-<2-(2,5-Dimethoxyphenyl)-2-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>-ethyl>-2-<<(1,1-dimethylethoxy)-carbonyl>-amino>-acetamid

Base Information

Chemical Name:<2R-(2α(R*),3aα,4α,7α,7aα)>-N-<2-(2,5-Dimethoxyphenyl)-2-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>-ethyl>-2-<<(1,1-dimethylethoxy)-carbonyl>-amino>-acetamid
CAS No.:133163-24-3
Molecular Formula:C₂₉H₄₄N₂O₇
Molecular Weight:532.678
Hs Code.:

<2R-(2α(R*),3aα,4α,7α,7aα)>-N-<2-(2,5-Dimethoxyphenyl)-2-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>-ethyl>-2-<<(1,1-dimethylethoxy)-carbonyl>-amino>-acetamid

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Chemical Property of <2R-(2α(R*),3aα,4α,7α,7aα)>-N-<2-(2,5-Dimethoxyphenyl)-2-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>-ethyl>-2-<<(1,1-dimethylethoxy)-carbonyl>-amino>-acetamid

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Technology Process of <2R-(2α(R*),3aα,4α,7α,7aα)>-N-<2-(2,5-Dimethoxyphenyl)-2-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>-ethyl>-2-<<(1,1-dimethylethoxy)-carbonyl>-amino>-acetamid

There total 2 articles about <2R-(2α(R*),3aα,4α,7α,7aα)>-N-<2-(2,5-Dimethoxyphenyl)-2-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>-ethyl>-2-<<(1,1-dimethylethoxy)-carbonyl>-amino>-acetamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 3392-07-2
tert-butyl N-{2-[(2,5-dioxopyrrolidin-1-yl)oxy]-2-oxoethyl}carbamate

: 133092-71-4
<2R-(2α(R*),3aα,4α,7α,7aα)>-2,5-Dimethoxy-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)-oxy>-benzolethanamin

: 133163-24-3
<2R-(2α(R*),3aα,4α,7α,7aα)>-N-<2-(2,5-Dimethoxyphenyl)-2-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>-ethyl>-2-<<(1,1-dimethylethoxy)-carbonyl>-amino>-acetamid

Guidance literature:: In tetrahydrofuran; for 0.25h; Ambient temperature;
DOI:10.1007/BF00807429

Reference yield: 82.0%

: 67084-40-6
1-(N-tert-butoxycarbonyl-glycyloxy)-1H-benzotriazole

: 133092-71-4
<2R-(2α(R*),3aα,4α,7α,7aα)>-2,5-Dimethoxy-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)-oxy>-benzolethanamin

: 133163-24-3
<2R-(2α(R*),3aα,4α,7α,7aα)>-N-<2-(2,5-Dimethoxyphenyl)-2-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>-ethyl>-2-<<(1,1-dimethylethoxy)-carbonyl>-amino>-acetamid

Guidance literature:: In dichloromethane; for 1h; Ambient temperature;
DOI:10.1007/BF00807429

Reference yield:

: 133163-24-3
<2R-(2α(R*),3aα,4α,7α,7aα)>-N-<2-(2,5-Dimethoxyphenyl)-2-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>-ethyl>-2-<<(1,1-dimethylethoxy)-carbonyl>-amino>-acetamid

: 133163-28-7,3092-17-9,43218-56-0
(S)-2-Amino-N-<2-(2,5-dimethoxyphenyl)-2-hydroxyethyl>-acetamid-hydrochlorid

: 133163-28-7,3092-17-9,43218-56-0
(R)-2-Amino-N-<2-(2,5-dimethoxyphenyl)-2-hydroxyethyl>-acetamid-hydrochlorid

Guidance literature:: With hydrogenchloride; In methanol; diethyl ether; at 40 ℃; for 0.0166667h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1007/BF00807429