Technology Process of C53H46N8O5S
There total 17 articles about C53H46N8O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: H2 / Pd/C / ethanol / 6 h / 20 °C
2: triethylamine / CH2Cl2 / -30 - 20 °C
3: CH2Cl2 / 20 °C
With
hydrogen; triethylamine;
palladium on activated charcoal;
In
ethanol; dichloromethane;
DOI:10.1016/j.bmc.2003.12.043
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine / 4 h / 20 °C
2: LiN3 / dimethylformamide / 4 h / 90 °C
3: H2 / Pd/C / ethanol / 6 h / 20 °C
4: triethylamine / CH2Cl2 / -30 - 20 °C
5: CH2Cl2 / 20 °C
With
pyridine; lithium azide; hydrogen; triethylamine;
palladium on activated charcoal;
In
ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2003.12.043
- Guidance literature:
-
Multi-step reaction with 7 steps
1: trifluoromethanesulfonic anhydride; pyridine / CH2Cl2 / -35 - 0 °C
2: aq. NaOH / dioxane; methanol / 0 °C
3: pyridine / 4 h / 20 °C
4: LiN3 / dimethylformamide / 4 h / 90 °C
5: H2 / Pd/C / ethanol / 6 h / 20 °C
6: triethylamine / CH2Cl2 / -30 - 20 °C
7: CH2Cl2 / 20 °C
With
pyridine; sodium hydroxide; lithium azide; hydrogen; trifluoromethanesulfonic acid anhydride; triethylamine;
palladium on activated charcoal;
In
1,4-dioxane; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2003.12.043
