1,2-Bis(2-mercapto-3,5-di-^tbutylanilino)ethan

Base Information

Chemical Name:1,2-Bis(2-mercapto-3,5-di-^tbutylanilino)ethan
CAS No.:113002-68-9
Molecular Formula:C₃₀H₄₈N₂S₂
Molecular Weight:500.857
Hs Code.:

1,2-Bis(2-mercapto-3,5-di-<sup>t</sup>butylanilino)ethan

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Chemical Property of 1,2-Bis(2-mercapto-3,5-di-^tbutylanilino)ethan

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Technology Process of 1,2-Bis(2-mercapto-3,5-di-^tbutylanilino)ethan

There total 5 articles about 1,2-Bis(2-mercapto-3,5-di-^tbutylanilino)ethan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112548-22-8
2-Mercapto-3,5-di-^tbutylanilin

: 113002-68-9
1,2-Bis(2-mercapto-3,5-di-^tbutylanilino)ethan

Guidance literature:: Multi-step reaction with 2 steps

1: 98.5 percent / methanol; H₂O

2: 1.) LiAlH₄, Na3)2>, 2.) LiAlH₄ / 1.) THF, room temperature, 1 h, 2.) MeOH

With lithium aluminium tetrahydride; sodium hexamethyldisilazane; In methanol; water;

Reference yield:

: 112548-21-7
2-Amino-5,7-di-^tbutylbenzthiazol

: 113002-68-9
1,2-Bis(2-mercapto-3,5-di-^tbutylanilino)ethan

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) KOH, 2.) glacial CH₃COOH / 1.) 2,3-butandiole, 3 h, 200 degC; 2.) heating

2: 98.5 percent / methanol; H₂O

3: 1.) LiAlH₄, Na3)2>, 2.) LiAlH₄ / 1.) THF, room temperature, 1 h, 2.) MeOH

With potassium hydroxide; lithium aluminium tetrahydride; sodium hexamethyldisilazane; acetic acid; In methanol; water;

Reference yield:

: 2380-36-1
3,5-di-tert-butylaniline

: 113002-68-9
1,2-Bis(2-mercapto-3,5-di-^tbutylanilino)ethan

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) glacial CH₃COOH, Br₂, 2.) KOH / 1.) 30 min., RT; 2.) MeOH, H₂O

2: 1.) KOH, 2.) glacial CH₃COOH / 1.) 2,3-butandiole, 3 h, 200 degC; 2.) heating

3: 98.5 percent / methanol; H₂O

4: 1.) LiAlH₄, Na3)2>, 2.) LiAlH₄ / 1.) THF, room temperature, 1 h, 2.) MeOH

With potassium hydroxide; lithium aluminium tetrahydride; bromine; sodium hexamethyldisilazane; acetic acid; In methanol; water;