acetic acid 3-acetylamino-6-benzyloxymethyl-5-[6-benzyloxymethyl-4,5-dihydroxy-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-tetrahydro-pyran-4-yl ester

Base Information

Chemical Name:acetic acid 3-acetylamino-6-benzyloxymethyl-5-[6-benzyloxymethyl-4,5-dihydroxy-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-tetrahydro-pyran-4-yl ester
CAS No.:497173-12-3
Molecular Formula:C₆₂H₇₃F₃N₂O₁₇
Molecular Weight:1175.26
Hs Code.:

acetic acid 3-acetylamino-6-benzyloxymethyl-5-[6-benzyloxymethyl-4,5-dihydroxy-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-tetrahydro-pyran-4-yl ester

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Chemical Property of acetic acid 3-acetylamino-6-benzyloxymethyl-5-[6-benzyloxymethyl-4,5-dihydroxy-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-tetrahydro-pyran-4-yl ester

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Technology Process of acetic acid 3-acetylamino-6-benzyloxymethyl-5-[6-benzyloxymethyl-4,5-dihydroxy-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-tetrahydro-pyran-4-yl ester

There total 2 articles about acetic acid 3-acetylamino-6-benzyloxymethyl-5-[6-benzyloxymethyl-4,5-dihydroxy-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-tetrahydro-pyran-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₅H₇₇F₃N₂O₁₇

: 497173-12-3
acetic acid 3-acetylamino-6-benzyloxymethyl-5-[6-benzyloxymethyl-4,5-dihydroxy-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-tetrahydro-pyran-4-yl ester

Guidance literature:: With trifluoroacetic acid;
DOI:10.1070/MC2002v012n04ABEH001591

Reference yield:

: 497173-10-1
C₆₃H₇₅F₃N₂O₁₆

: 497173-12-3
acetic acid 3-acetylamino-6-benzyloxymethyl-5-[6-benzyloxymethyl-4,5-dihydroxy-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-tetrahydro-pyran-4-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: CF₃COOH

With pyridine; trifluoroacetic acid;
DOI:10.1070/MC2002v012n04ABEH001591

Reference yield: 89.0%

: 64-19-7,77671-22-8
acetic acid

: 497173-12-3
acetic acid 3-acetylamino-6-benzyloxymethyl-5-[6-benzyloxymethyl-4,5-dihydroxy-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-tetrahydro-pyran-4-yl ester

: acetic acid 6-{4-acetoxy-5-acetylamino-2-benzyloxymethyl-6-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-tetrahydro-pyran-3-yloxy}-2-benzyloxymethyl-4-hydroxy-5-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester

Guidance literature:: acetic acid 3-acetylamino-6-benzyloxymethyl-5-[6-benzyloxymethyl-4,5-dihydroxy-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-tetrahydro-pyran-4-yl ester; With toluene-4-sulfonic acid; Triethyl orthoacetate;

acetic acid;
DOI:10.1070/MC2002v012n04ABEH001591