dicarbonylchloro(1,3-di-p-tolyltriazene)iridium

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Chemical Name:dicarbonylchloro(1,3-di-p-tolyltriazene)iridium
CAS No.:286839-76-7
Molecular Formula:C₁₆H₁₅ClIrN₃O₂
Molecular Weight:508.987
Hs Code.:

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Chemical Property of dicarbonylchloro(1,3-di-p-tolyltriazene)iridium

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Technology Process of dicarbonylchloro(1,3-di-p-tolyltriazene)iridium

There total 1 articles about dicarbonylchloro(1,3-di-p-tolyltriazene)iridium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 115680-45-0
chloro(η-4-cyclo-octa-1,5-diene)(1,3-di-p-tolyltriazene)iridium

: 286839-76-7,115680-46-1
dicarbonylchloro(1,3-di-p-tolyltriazene)iridium

Guidance literature:: With carbon monoxide; In dichloromethane; CO gas was slowly bubbled for 15 min through a soln. of Ir-complex in CH2Cl2, hexane was added under N2; concd. in vac.; elem. anal.;
DOI:10.1039/DT9870002737

Reference yield: 40.0%

: 286839-76-7,115680-46-1
dicarbonylchloro(1,3-di-p-tolyltriazene)iridium

: tetracarbonyl-di-μ-(di-p-tolyltriazenido)-di-iridium-n-hexane (2/1)

Guidance literature:: With hexane; triethylamine; In dichloromethane; to a cooled (-78°C) soln. of Ir-complex in CH2Cl2 was added Et3N, warmed to room temp., stirred for 4 h under N2; solvent removed in vac., the residue extd. with n-hexane, the extract was evapd., placed on an Al-n-hexane chromy. column, n-hexane was used as eluent, collected, concd., cooled to -10°C; elem. anal.;
DOI:10.1039/DT9870002737