Acetic acid (2S,3R,4S,5S,6R)-4,5-diacetoxy-2-[(S)-1,5-dimethyl-1-((S)-4-methyl-cyclohex-3-enyl)-4-oxo-hex-5-enyloxy]-6-methyl-tetrahydro-pyran-3-yl ester

Base Information

Chemical Name:Acetic acid (2S,3R,4S,5S,6R)-4,5-diacetoxy-2-[(S)-1,5-dimethyl-1-((S)-4-methyl-cyclohex-3-enyl)-4-oxo-hex-5-enyloxy]-6-methyl-tetrahydro-pyran-3-yl ester
CAS No.:126616-74-8
Molecular Formula:C₂₇H₄₀O₉
Molecular Weight:508.609
Hs Code.:

Acetic acid (2S,3R,4S,5S,6R)-4,5-diacetoxy-2-[(S)-1,5-dimethyl-1-((S)-4-methyl-cyclohex-3-enyl)-4-oxo-hex-5-enyloxy]-6-methyl-tetrahydro-pyran-3-yl ester

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Chemical Property of Acetic acid (2S,3R,4S,5S,6R)-4,5-diacetoxy-2-[(S)-1,5-dimethyl-1-((S)-4-methyl-cyclohex-3-enyl)-4-oxo-hex-5-enyloxy]-6-methyl-tetrahydro-pyran-3-yl ester

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Technology Process of Acetic acid (2S,3R,4S,5S,6R)-4,5-diacetoxy-2-[(S)-1,5-dimethyl-1-((S)-4-methyl-cyclohex-3-enyl)-4-oxo-hex-5-enyloxy]-6-methyl-tetrahydro-pyran-3-yl ester

There total 3 articles about Acetic acid (2S,3R,4S,5S,6R)-4,5-diacetoxy-2-[(S)-1,5-dimethyl-1-((S)-4-methyl-cyclohex-3-enyl)-4-oxo-hex-5-enyloxy]-6-methyl-tetrahydro-pyran-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79197-23-2,84847-69-8
Acetic acid (2S,3R,4S,5S,6R)-4,5-diacetoxy-2-[(S)-1,5-dimethyl-1-((S)-4-methyl-cyclohex-3-enyl)-hex-4-enyloxy]-6-methyl-tetrahydro-pyran-3-yl ester

: 126616-74-8
Acetic acid (2S,3R,4S,5S,6R)-4,5-diacetoxy-2-[(S)-1,5-dimethyl-1-((S)-4-methyl-cyclohex-3-enyl)-4-oxo-hex-5-enyloxy]-6-methyl-tetrahydro-pyran-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) oxygen, h*ν, 2) dimethyl sulphide / 1) Rose Bengale / 1) iso-PrOH, sunshine, 4 h

2: 136 mg / PDC / CH₂Cl₂ / 5 h / Ambient temperature

With dipyridinium dichromate; dimethylsulfide; oxygen; 4,5,6,7-tetrachloro-2',4',5',7'-tetraiodofluorescein disodium salt; In dichloromethane;
DOI:10.1016/0031-9422(90)85135-3

Reference yield:

: 126582-68-1
Acetic acid (2S,3R,4S,5S,6R)-4,5-diacetoxy-2-[(S)-4-hydroxy-1,5-dimethyl-1-((S)-4-methyl-cyclohex-3-enyl)-hex-5-enyloxy]-6-methyl-tetrahydro-pyran-3-yl ester

: 126616-74-8
Acetic acid (2S,3R,4S,5S,6R)-4,5-diacetoxy-2-[(S)-1,5-dimethyl-1-((S)-4-methyl-cyclohex-3-enyl)-4-oxo-hex-5-enyloxy]-6-methyl-tetrahydro-pyran-3-yl ester

Guidance literature:: With dipyridinium dichromate; In dichloromethane; for 5h; Ambient temperature;
DOI:10.1016/0031-9422(90)85135-3

Reference yield:

: 79197-23-2,84847-69-8
Acetic acid (2S,3R,4S,5S,6R)-4,5-diacetoxy-2-[(S)-1,5-dimethyl-1-((S)-4-methyl-cyclohex-3-enyl)-hex-4-enyloxy]-6-methyl-tetrahydro-pyran-3-yl ester

: 126646-28-4
Acetic acid (2S,3R,4S,5S,6R)-4,5-diacetoxy-6-methyl-2-[(S)-1-methyl-1-((S)-4-methyl-cyclohex-3-enyl)-4-oxo-butoxy]-tetrahydro-pyran-3-yl ester

: 126616-74-8
Acetic acid (2S,3R,4S,5S,6R)-4,5-diacetoxy-2-[(S)-1,5-dimethyl-1-((S)-4-methyl-cyclohex-3-enyl)-4-oxo-hex-5-enyloxy]-6-methyl-tetrahydro-pyran-3-yl ester

Guidance literature:: With pyridine; oxygen; acetic anhydride; 4,5,6,7-tetrachloro-2',4',5',7'-tetraiodofluorescein disodium salt; Yield given. Multistep reaction. Yields of byproduct given; 1) iso-PrOH, sunshine, 4 h, 2) room temperature, 12 h;
DOI:10.1016/0031-9422(90)85135-3