[Fe(Cl)(CO)(P(OEt)3)4]BPh₄

Base Information

Chemical Name:[Fe(Cl)(CO)(P(OEt)3)4]BPh₄
CAS No.:100112-87-6
Molecular Formula:C₂₄H₂₀B*C₂₅H₆₀ClFeO₁₃P₄
Molecular Weight:1103.17
Hs Code.:

Synonyms:

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Chemical Property of [Fe(Cl)(CO)(P(OEt)3)4]BPh₄

Chemical Property:

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Technology Process of [Fe(Cl)(CO)(P(OEt)3)4]BPh₄

There total 2 articles about [Fe(Cl)(CO)(P(OEt)3)4]BPh₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 143-66-8
sodium tetraphenyl borate

: iron(II) chloride

: 122-52-1
triethyl phosphite

: 100112-87-6,104319-58-6,104319-59-7
FeCl(CO)(P(OC₂H₅)3)4⁽¹⁺⁾*B(C₆H₅)4^(1-) = [FeCl(CO)(P(OC₂H₅)3)4]B(C₆H₅)4

: 100112-87-6,104319-58-6,104319-59-7
FeCl(CO)(P(OC₂H₅)3)4⁽¹⁺⁾*B(C₆H₅)4^(1-) = [FeCl(CO)(P(OC₂H₅)3)4]B(C₆H₅)4

Guidance literature:: With CO; In ethanol; under an inert atmosphere; phosphite added to a soln. of FeCl2 and stirred for 3 h; allowed to stand under CO for 2 h; filtered; NaB(C6H5)4 added; pptd.; washed with alcohol; dried in vacuo; mixed with ethanol or methanol and acetone at room temp.; cooled slowly to -20°C; washed; dried; concentrated; warmed to 50°C; cooled to -30°C; washedwith alcohol; dried; elem. anal.;
DOI:10.1039/DT9860000329

Reference yield:

: 143-66-8
sodium tetraphenyl borate

: iron(II) chloride

: 122-52-1
triethyl phosphite

: 100112-87-6,104319-58-6,104319-59-7
FeCl(CO)(P(OC₂H₅)3)4⁽¹⁺⁾*B(C₆H₅)4^(1-) = [FeCl(CO)(P(OC₂H₅)3)4]B(C₆H₅)4

: 100112-87-6,104319-58-6,104319-59-7
FeCl(CO)(P(OC₂H₅)3)4⁽¹⁺⁾*B(C₆H₅)4^(1-) = [FeCl(CO)(P(OC₂H₅)3)4]B(C₆H₅)4

Guidance literature:: With CO; In ethanol; under an inert atmosphere; phosphite added to a soln. of FeCl2 and stirred for 3 h; allowed to stand under CO for 2 h; filtered; NaB(C6H5)4 added; pptd.; washed with alcohol; dried in vacuo; mixed with ethanol or methanol and acetone at room temp.; cooled slowly to -20°C; washed; dried; concentrated; warmed to 50°C; cooled to -30°C; washedwith alcohol; dried; elem. anal.;
DOI:10.1039/DT9860000329

Reference yield:

: 100112-87-6
[Fe(Cl)(CO)(P(OEt)3)4]BPh₄

: 95738-79-7
trans-{FeH(CO)(P(OEt)3)4}BPh₄

Guidance literature:: With Zn; In acetonitrile; under inert atmosphere; zinc dust in excess added to a soln. of Fe-complex; stirred until the soln. turned colorless; filtered; evapd.; stirred with ethanol or methanol for 1 h; crystd. from alcohol; elem. anal.;