C₆₃H₇₆N₄O₁₁S

Base Information

• Chemical Name: C₆₃H₇₆N₄O₁₁S
• CAS No.: 632329-10-3
• Molecular Formula: C₆₃H₇₆N₄O₁₁S
• Molecular Weight: 1097.38
• Mol file: 632329-10-3.mol

Synonyms:

Chemical Property of C₆₃H₇₆N₄O₁₁S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₃H₇₆N₄O₁₁S

There total 11 articles about C₆₃H₇₆N₄O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C37H53N2O3Si(1+)*Br(1-) → C63H76N4O11S (632329-10-3)

Guidance literature:

Multi-step reaction with 6 steps

1.1: 7.619 g / Et₃N / methanol / 144 h / Heating

2.1: 92 percent / aq. Bu₄NF / tetrahydrofuran / 2 h

3.1: 95 percent / Et₃N / CH₂Cl₂ / 0 - 20 °C

4.1: Et₃N / CH₂Cl₂ / 0.08 h / 0 °C

4.2: tert-butyl hypochlorite / CH₂Cl₂ / 0.17 h / 0 °C

5.1: HBF₄*Et₂O; AgBF₄ / acetone / 0.5 h

6.1: 0.231 g / KBH₄; AcOH / 0.33 h

With tetrafluoroboric acid diethyl ether; silver tetrafluoroborate; potassium borohydride; tetrabutyl ammonium fluoride; acetic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; acetone;

DOI:10.1039/b209990j

Reference yield:

1-(2-cyanoethyl)-1-formylcyclohexane (58886-81-0) → C63H76N4O11S (632329-10-3)

Guidance literature:

Multi-step reaction with 11 steps

1.1: 98 percent / NaBH₄ / methanol / 1 h / 0 °C

2.1: Et₃N / CH₂Cl₂ / 0.25 h / 0 °C

2.2: 75 percent / DMAP / CH₂Cl₂ / 16 h / 20 °C

3.1: 70 percent / DIBAL-H / CH₂Cl₂ / 6 h / -78 °C

4.1: tetrahydrofuran / 24 h / 20 °C

5.1: tetrahydrofuran / 24 h / Heating

6.1: 7.619 g / Et₃N / methanol / 144 h / Heating

7.1: 92 percent / aq. Bu₄NF / tetrahydrofuran / 2 h

8.1: 95 percent / Et₃N / CH₂Cl₂ / 0 - 20 °C

9.1: Et₃N / CH₂Cl₂ / 0.08 h / 0 °C

9.2: tert-butyl hypochlorite / CH₂Cl₂ / 0.17 h / 0 °C

10.1: HBF₄*Et₂O; AgBF₄ / acetone / 0.5 h

11.1: 0.231 g / KBH₄; AcOH / 0.33 h

With tetrafluoroboric acid diethyl ether; sodium tetrahydroborate; silver tetrafluoroborate; potassium borohydride; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; acetic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; acetone;

DOI:10.1039/b209990j

Reference yield:

1-[tert-butyldimethylsilyloxymethyl]-1-(3-propanalyl)-cyclohexane (632329-00-1) → C63H76N4O11S (632329-10-3)

Guidance literature:

Multi-step reaction with 8 steps

1.1: tetrahydrofuran / 24 h / 20 °C

2.1: tetrahydrofuran / 24 h / Heating

3.1: 7.619 g / Et₃N / methanol / 144 h / Heating

4.1: 92 percent / aq. Bu₄NF / tetrahydrofuran / 2 h

5.1: 95 percent / Et₃N / CH₂Cl₂ / 0 - 20 °C

6.1: Et₃N / CH₂Cl₂ / 0.08 h / 0 °C

6.2: tert-butyl hypochlorite / CH₂Cl₂ / 0.17 h / 0 °C

7.1: HBF₄*Et₂O; AgBF₄ / acetone / 0.5 h

8.1: 0.231 g / KBH₄; AcOH / 0.33 h

With tetrafluoroboric acid diethyl ether; silver tetrafluoroborate; potassium borohydride; tetrabutyl ammonium fluoride; acetic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; acetone;

DOI:10.1039/b209990j

upstream raw materials:

1-(2-cyanoethyl)-1-formylcyclohexane

3-(1-(hydroxymethyl)cyclohexyl)propanenitrile

1-[tert-butyldimethylsilyloxymethyl]-1-(3-propanalyl)-cyclohexane

1-[tert-butyl-dimethylsilyloxymethyl]-1-(2-cyanoethyl)-cyclohexane