1-(p-trifluoromethyl)phenyl-3,4-dimethyl-Δ³-phospholen oxide

Base Information

Chemical Name:1-(p-trifluoromethyl)phenyl-3,4-dimethyl-Δ³-phospholen oxide
CAS No.:82217-41-2
Molecular Formula:C₁₃H₁₄F₃OP
Molecular Weight:274.223
Hs Code.:

1-(p-trifluoromethyl)phenyl-3,4-dimethyl-Δ<sup>3</sup>-phospholen oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(p-trifluoromethyl)phenyl-3,4-dimethyl-Δ³-phospholen oxide

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Technology Process of 1-(p-trifluoromethyl)phenyl-3,4-dimethyl-Δ³-phospholen oxide

There total 2 articles about 1-(p-trifluoromethyl)phenyl-3,4-dimethyl-Δ³-phospholen oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82217-36-5
1,1-dibromo-3,4-dimethyl-Δ³-phospholenium bromide

: 82217-41-2
1-(p-trifluoromethyl)phenyl-3,4-dimethyl-Δ³-phospholen oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / methanol, triethylamine / CH₂Cl₂

2: 1.) magnesium turnings, 1,2-dibromoethane / 1.) THF, 1 h; 2.) diethyl ether, RT, overnight

With methanol; magnesium; ethylene dibromide; triethylamine; In dichloromethane;
DOI:10.1039/P29820000205

Reference yield:

: 402-43-7
p-trifluoromethylphenyl bromide

: 873-14-3
1-bromo-3,4-dimethyl-Δ³-phospholen oxide

: 82217-41-2
1-(p-trifluoromethyl)phenyl-3,4-dimethyl-Δ³-phospholen oxide

Guidance literature:: With magnesium; ethylene dibromide; Yield given. Multistep reaction; 1.) THF, 1 h; 2.) diethyl ether, RT, overnight;
DOI:10.1039/P29820000205