(+/-)-2-(1-benzylindazol-3-yl)cyclohexanol

Base Information

Chemical Name:(+/-)-2-(1-benzylindazol-3-yl)cyclohexanol
CAS No.:103595-01-3
Molecular Formula:C₂₀H₂₂N₂O
Molecular Weight:306.407
Hs Code.:

Synonyms:

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Chemical Property of (+/-)-2-(1-benzylindazol-3-yl)cyclohexanol

Chemical Property:

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Technology Process of (+/-)-2-(1-benzylindazol-3-yl)cyclohexanol

There total 13 articles about (+/-)-2-(1-benzylindazol-3-yl)cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95-20-5
2-methyl-1H-indole

: 103595-01-3
(+/-)-2-(1-benzylindazol-3-yl)cyclohexanol

Guidance literature:: Multi-step reaction with 6 steps

2: 71 percent / sodium periodate / H₂O; methanol / 72 h / Ambient temperature

3: 85 percent / cc. HCl / H₂O; ethanol / 3 h / Heating

4: 1.) cc HCl, sodium nitrite 2.) sodium azide / 1.) aceton, water, 30 min, 0 deg C 2.) water, 30 min

5: 40 percent / hydrazine hydrate / acetic acid; ethanol / 5 h / Heating

6: 1.) sodium hydride / 1.) THF, 0 deg C 2.) 30 min, 0 deg C, 1h, 40 deg C, THF

With hydrogenchloride; sodium periodate; sodium azide; sodium hydride; hydrazine hydrate; sodium nitrite; In methanol; ethanol; water; acetic acid;
DOI:10.1039/P19850000001

Reference yield:

: 286-20-4
cyclohexane-1,2-epoxide

: 103595-01-3
(+/-)-2-(1-benzylindazol-3-yl)cyclohexanol

Guidance literature:: Multi-step reaction with 6 steps

2: 71 percent / sodium periodate / H₂O; methanol / 72 h / Ambient temperature

3: 85 percent / cc. HCl / H₂O; ethanol / 3 h / Heating

4: 1.) cc HCl, sodium nitrite 2.) sodium azide / 1.) aceton, water, 30 min, 0 deg C 2.) water, 30 min

5: 40 percent / hydrazine hydrate / acetic acid; ethanol / 5 h / Heating

6: 1.) sodium hydride / 1.) THF, 0 deg C 2.) 30 min, 0 deg C, 1h, 40 deg C, THF

With hydrogenchloride; sodium periodate; sodium azide; sodium hydride; hydrazine hydrate; sodium nitrite; In methanol; ethanol; water; acetic acid;
DOI:10.1039/P19850000001

Reference yield:

: 32605-77-9
(+/-)-2-(2-methylindol-3-yl)cyclohexanone

: 103595-01-3
(+/-)-2-(1-benzylindazol-3-yl)cyclohexanol

Guidance literature:: Multi-step reaction with 6 steps

1: sodium borohydride / ethanol / 1 h / Heating

2: 71 percent / sodium periodate / H₂O; methanol / 72 h / Ambient temperature

3: 85 percent / cc. HCl / H₂O; ethanol / 3 h / Heating

4: 1.) cc HCl, sodium nitrite 2.) sodium azide / 1.) aceton, water, 30 min, 0 deg C 2.) water, 30 min

5: 40 percent / hydrazine hydrate / acetic acid; ethanol / 5 h / Heating

6: 1.) sodium hydride / 1.) THF, 0 deg C 2.) 30 min, 0 deg C, 1h, 40 deg C, THF

With hydrogenchloride; sodium tetrahydroborate; sodium periodate; sodium azide; sodium hydride; hydrazine hydrate; sodium nitrite; In methanol; ethanol; water; acetic acid;
DOI:10.1039/P19850000001