2-[(2-Fluorophenyl)thio]-5-nitrobenzenemethanol

Base Information

Chemical Name:2-[(2-Fluorophenyl)thio]-5-nitrobenzenemethanol
CAS No.:73129-15-4
Molecular Formula:C₁₃H₁₀FNO₃S
Molecular Weight:279.292
Hs Code.:
DSSTox Substance ID:DTXSID201244514

Synonyms:2-[(2-Fluorophenyl)thio]-5-nitrobenzenemethanol;DTXSID201244514;AKOS013127010;73129-15-4

Suppliers and Price of 2-[(2-Fluorophenyl)thio]-5-nitrobenzenemethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(2-Fluorophenyl)thio]-5-nitrobenzenemethanol

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:279.03654252
Heavy Atom Count:19
Complexity:313

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C(=C1)F)SC2=C(C=C(C=C2)[N+](=O)[O-])CO

Technology Process of 2-[(2-Fluorophenyl)thio]-5-nitrobenzenemethanol

There total 1 articles about 2-[(2-Fluorophenyl)thio]-5-nitrobenzenemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2557-78-0
2-fluorothiophenol

: 73129-15-4
[2-(2-Fluoro-phenylsulfanyl)-5-nitro-phenyl]-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: Cu, aq. KOH

2: NaBH₄ / tetrahydrofuran

With potassium hydroxide; sodium tetrahydroborate; copper; In tetrahydrofuran;
DOI:10.1135/cccc19792139

Reference yield:

: 73129-15-4
[2-(2-Fluoro-phenylsulfanyl)-5-nitro-phenyl]-methanol

: 73129-19-8
5-chloro-2-(2-fluorophenylthio)benzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: SnCl₂ / diethyl ether

2: (i) NaNO₂, aq. HCl, (ii) CuCl

With tin(ll) chloride; In diethyl ether;
DOI:10.1135/cccc19792139

Reference yield:

: 73129-15-4
[2-(2-Fluoro-phenylsulfanyl)-5-nitro-phenyl]-methanol

: 73129-20-1
4-Chloro-2-chloromethyl-1-(2-fluoro-phenylsulfanyl)-benzene

Guidance literature:: Multi-step reaction with 3 steps

1: SnCl₂ / diethyl ether

2: (i) NaNO₂, aq. HCl, (ii) CuCl

3: SOCl₂, Py / benzene

With pyridine; thionyl chloride; tin(ll) chloride; In diethyl ether; benzene;
DOI:10.1135/cccc19792139