mesitylbromo{1,2-bis(diisopropylphosphino)ethane}iron(II)

Base Information

Chemical Name:mesitylbromo{1,2-bis(diisopropylphosphino)ethane}iron(II)
CAS No.:106905-35-5
Molecular Formula:C₂₃H₄₃BrFeP₂
Molecular Weight:517.293
Hs Code.:

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Chemical Property of mesitylbromo{1,2-bis(diisopropylphosphino)ethane}iron(II)

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Technology Process of mesitylbromo{1,2-bis(diisopropylphosphino)ethane}iron(II)

There total 1 articles about mesitylbromo{1,2-bis(diisopropylphosphino)ethane}iron(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 106905-37-7
dibromo{1,2-bis(diisopropylphosphino)ethane}iron(II)

: 2633-66-1
2-mesitylmagnesium bromide

: 106905-35-5
mesitylbromo{1,2-bis(diisopropylphosphino)ethane}iron(II)

Guidance literature:: In tetrahydrofuran; byproducts: MgBr2; THF soln. of MesMgBr was added to a cold (-78°C) soln. of FeBr2(dippe) in THF, mixt. was stirred for 1 h at -78°C under Ar; warmed to 0°C, evapd., residue was extd. with toluene, ext. was filtered, concd., cooled to -20°C; elem. anal.;
DOI:10.1021/om00147a014

Reference yield: 38.0%

: 106905-35-5
iron(mesityl)Br{1,2-bis(diisopropylphosphino)ethane}iron(II)

: 111291-21-5
iron(η2-CO-mesityl)Br(carbonyl){1,2-bis(diisopropylphosphino)ethane}iron(II)

Guidance literature:: With CO; In toluene; Dissolving, pressurizing with CO (to 3 atm), the yellow soln. immediately turns dark orange, stirring (2 h).; Filtn., concg., cooling (to -20°C).;