5-acetyl-5H,6H-11,12-didehydrodibenzo[b,f]azocin

Base Information

Chemical Name:5-acetyl-5H,6H-11,12-didehydrodibenzo[b,f]azocin
CAS No.:1421353-86-7
Molecular Formula:C₁₇H₁₃NO
Molecular Weight:247.296
Hs Code.:

Synonyms:

Suppliers and Price of 5-acetyl-5H,6H-11,12-didehydrodibenzo[b,f]azocin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of 5-acetyl-5H,6H-11,12-didehydrodibenzo[b,f]azocin

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-acetyl-5H,6H-11,12-didehydrodibenzo[b,f]azocin

There total 6 articles about 5-acetyl-5H,6H-11,12-didehydrodibenzo[b,f]azocin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98090-02-9
N-acetyl-5,6-dihydrodibenzo[b,f]azocine

: 1421353-86-7
5-acetyl-5H,6H-11,12-didehydrodibenzo[b,f]azocin

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium hydrobromide perbromide / dichloromethane / 6.5 h / 20 °C / Darkness

2: potassium tert-butylate / tetrahydrofuran / 1.5 h / 0 - 20 °C

With potassium tert-butylate; pyridinium hydrobromide perbromide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201302502

Reference yield:

: C₁₇H₁₅Br₂NO

: 1421353-86-7
5-acetyl-5H,6H-11,12-didehydrodibenzo[b,f]azocin

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; for 1.5h;
DOI:10.1002/chem.201302502

Reference yield:

: 1021-91-6
N-[tricyclo[9.4.0.0^3,8]pentadeca-1⁽¹¹⁾,3,5,7,9,12,14-heptaen-2-ylidene]hydroxylamine

: 1421353-86-7
5-acetyl-5H,6H-11,12-didehydrodibenzo[b,f]azocin

Guidance literature:: Multi-step reaction with 5 steps

1: polyphosphoric acid / 1.5 h / 125 °C / Inert atmosphere

2: lithium aluminium tetrahydride / diethyl ether / 40 h / Inert atmosphere; Reflux

3: pyridine / dichloromethane / 1 h / 0 - 20 °C / Molecular sieve

4: pyridinium hydrobromide perbromide / dichloromethane / 6.5 h / 20 °C / Darkness

5: potassium tert-butylate / tetrahydrofuran / 1.5 h / 0 - 20 °C

With pyridine; lithium aluminium tetrahydride; potassium tert-butylate; pyridinium hydrobromide perbromide; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1002/chem.201302502