(4R,5S,6S)-(p-nitrobenzyl) 3-[[(3S,5S)-1-(-p-nitrobenzyloxycarbonyl)-5-(lithium carboxylato)-3-pyrrolidinyl]thio]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

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Chemical Name:(4R,5S,6S)-(p-nitrobenzyl) 3-[[(3S,5S)-1-(-p-nitrobenzyloxycarbonyl)-5-(lithium carboxylato)-3-pyrrolidinyl]thio]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate
CAS No.:903569-60-8
Molecular Formula:C₃₀H₂₉N₄O₁₂S*Li
Molecular Weight:676.587
Hs Code.:

(4R,5S,6S)-(p-nitrobenzyl) 3-[[(3S,5S)-1-(-p-nitrobenzyloxycarbonyl)-5-(lithium carboxylato)-3-pyrrolidinyl]thio]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

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Chemical Property of (4R,5S,6S)-(p-nitrobenzyl) 3-[[(3S,5S)-1-(-p-nitrobenzyloxycarbonyl)-5-(lithium carboxylato)-3-pyrrolidinyl]thio]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

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Technology Process of (4R,5S,6S)-(p-nitrobenzyl) 3-[[(3S,5S)-1-(-p-nitrobenzyloxycarbonyl)-5-(lithium carboxylato)-3-pyrrolidinyl]thio]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

There total 1 articles about (4R,5S,6S)-(p-nitrobenzyl) 3-[[(3S,5S)-1-(-p-nitrobenzyloxycarbonyl)-5-(lithium carboxylato)-3-pyrrolidinyl]thio]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 903569-57-3
(4R,5S,6S)-(p-nitrobenzyl) 3-[[(3S,5S)-1-(p-nitrobenzyloxycarbonyl)-5-carboxy-3-pyrrolidinyl]thio]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

: 903569-60-8
(4R,5S,6S)-(p-nitrobenzyl) 3-[[(3S,5S)-1-(-p-nitrobenzyloxycarbonyl)-5-(lithium carboxylato)-3-pyrrolidinyl]thio]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

Guidance literature:: With lithium 2-ethylhexanoate; In ethyl acetate; at 0 - 4 ℃; for 15.5h;

Reference yield:

: 903569-60-8
(4R,5S,6S)-(p-nitrobenzyl) 3-[[(3S,5S)-1-(-p-nitrobenzyloxycarbonyl)-5-(lithium carboxylato)-3-pyrrolidinyl]thio]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

: C₃₀H₂₉ClN₄O₁₁S

Guidance literature:: With pivaloyl chloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at -30 - -20 ℃; Product distribution / selectivity;